Bis(4-methyl-3-nitrophenyl)diazene 1-oxide

Base Information

• Chemical Name: Bis(4-methyl-3-nitrophenyl)diazene 1-oxide
• CAS No.: 5679-89-0
• Molecular Formula: C14H12N4O5
• Molecular Weight: 316.273
• Mol file: 5679-89-0.mol

Synonyms:4,4'-Dimethyl-3,3'-dinitroazoxybenzene;4,4'-Dimethyl-3,3'-dinitro-azoxybenzol;p,p'-Azoxytoluene,3,3'-dinitro;2,2'-Dinitro-4,4'-azoxytoluene;3.3'-Dinitro-4.4'-dimethyl-azoxybenzol;

Chemical Property of Bis(4-methyl-3-nitrophenyl)diazene 1-oxide

Chemical Property:

• Vapor Pressure: 1.16E-09mmHg at 25°C
• Melting Point: 167-170°C
• Boiling Point: 500.6°C at 760 mmHg
• Flash Point: 256.5°C
• PSA: 132.75000
• Density: 1.41g/cm³
• LogP: 5.61510
• Storage Temp.: Hygroscopic, Refrigerator, under inert atmosphere
• Solubility.: DMSO

Purity/Quality:

99% ^*data from raw suppliers

2,2''-Dinitro-4,4''-azoxytoluene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2,2''-Dinitro-4,4''-azoxytoluene is a metaboite of 2,4-dinitrotoluene by Salmonella typhimurium strains.

Technology Process of Bis(4-methyl-3-nitrophenyl)diazene 1-oxide

There total 13 articles about Bis(4-methyl-3-nitrophenyl)diazene 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-dinitrotoluene (121-14-2) → 4-Methyl-3-nitroanilin (119-32-4) + 2,2'-Dinitro-4,4'-azoxytoluene (5679-89-0)

Guidance literature:

With pyridine; hydrogen sulfide;

Reference yield:

sulfuric acid (7664-93-9) + 4-hydroxylamino-2-nitrotoluene (43192-03-6) → 4-Methyl-3-nitroanilin (119-32-4) + 2,2'-Dinitro-4,4'-azoxytoluene (5679-89-0)

Guidance literature:

Reference yield:

2,4-dinitrotoluene (121-14-2) + sulfuric acid (7664-93-9) → 4-methylbenzene-1,3-diamine (95-80-7,71111-07-4) + 4-Methyl-3-nitroanilin (119-32-4) + 2,2'-Dinitro-4,4'-azoxytoluene (5679-89-0)

Guidance literature:

bei der elektrolytischen Reduktion;

upstream raw materials:

piperidine

2,4-dinitrotoluene

2-hydroxy-2-phenylacetophenone

benzene