(S)-3-((S)-2-Amino-4-methylsulfanyl-butyrylamino)-N-((S)-1-carbamoyl-2-phenyl-ethyl)-succinamic acid tert-butyl ester; hydrochloride

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Chemical Name:(S)-3-((S)-2-Amino-4-methylsulfanyl-butyrylamino)-N-((S)-1-carbamoyl-2-phenyl-ethyl)-succinamic acid tert-butyl ester; hydrochloride
CAS No.:5609-54-1
Molecular Formula:C₂₂H₃₄N₄O₅S*ClH
Molecular Weight:503.063
Hs Code.:

Synonyms:(S)-3-((S)-2-Amino-4-methylsulfanyl-butyrylamino)-N-((S)-1-carbamoyl-2-phenyl-ethyl)-succinamic acid tert-butyl ester; hydrochloride

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Chemical Property of (S)-3-((S)-2-Amino-4-methylsulfanyl-butyrylamino)-N-((S)-1-carbamoyl-2-phenyl-ethyl)-succinamic acid tert-butyl ester; hydrochloride

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Technology Process of (S)-3-((S)-2-Amino-4-methylsulfanyl-butyrylamino)-N-((S)-1-carbamoyl-2-phenyl-ethyl)-succinamic acid tert-butyl ester; hydrochloride

There total 4 articles about (S)-3-((S)-2-Amino-4-methylsulfanyl-butyrylamino)-N-((S)-1-carbamoyl-2-phenyl-ethyl)-succinamic acid tert-butyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 62056-70-6
Nα-diphenylphosphinylmethionyl(β-t-butyl)aspartylphenylalanine amide

: 5609-54-1
(S)-3-((S)-2-Amino-4-methylsulfanyl-butyrylamino)-N-((S)-1-carbamoyl-2-phenyl-ethyl)-succinamic acid tert-butyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; In water; for 5h; Ambient temperature;

Reference yield:

: 5241-67-8
H-Asp(O-tBu)-Phe-NH₂

: 5609-54-1
(S)-3-((S)-2-Amino-4-methylsulfanyl-butyrylamino)-N-((S)-1-carbamoyl-2-phenyl-ethyl)-succinamic acid tert-butyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / N-hydroxysuccinimide, DCC / CH₂Cl₂ / 1.) 0 deg C, 2 h, 2.) room temperature, overnight

2: 70 percent / 4M HCl / H₂O; various solvent(s) / 5 h / Ambient temperature

With hydrogenchloride; 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In dichloromethane; water;

Reference yield:

: 62056-82-0
Nα-dipnenylphosphinylmethionine

: 5609-54-1
(S)-3-((S)-2-Amino-4-methylsulfanyl-butyrylamino)-N-((S)-1-carbamoyl-2-phenyl-ethyl)-succinamic acid tert-butyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / N-hydroxysuccinimide, DCC / CH₂Cl₂ / 1.) 0 deg C, 2 h, 2.) room temperature, overnight

2: 70 percent / 4M HCl / H₂O; various solvent(s) / 5 h / Ambient temperature

With hydrogenchloride; 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In dichloromethane; water;