N-[(1S,2R)-2-((2R)-2-hydroxy-phenylacetamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

Base Information

Chemical Name:N-[(1S,2R)-2-((2R)-2-hydroxy-phenylacetamido)cyclohexanecarboxy]-α-L-fucopyranosylamine
CAS No.:1329602-79-0
Molecular Formula:C₂₁H₃₀N₂O₇
Molecular Weight:422.478
Hs Code.:

Synonyms:N-[(1S,2R)-2-((2R)-2-hydroxy-phenylacetamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

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Chemical Property of N-[(1S,2R)-2-((2R)-2-hydroxy-phenylacetamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

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Technology Process of N-[(1S,2R)-2-((2R)-2-hydroxy-phenylacetamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

There total 3 articles about N-[(1S,2R)-2-((2R)-2-hydroxy-phenylacetamido)cyclohexanecarboxy]-α-L-fucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: C₂₉H₃₈N₂O₁₁

: 1329602-79-0
N-[(1S,2R)-2-((2R)-2-hydroxy-phenylacetamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

Guidance literature:: With methanol; sodium methylate; at 20 ℃; Inert atmosphere;
DOI:10.1039/c1ob05573a

Reference yield:

: 51019-43-3
(R)-(-)-O-acetylmandelic acid

: 1329602-79-0
N-[(1S,2R)-2-((2R)-2-hydroxy-phenylacetamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / toluene / 3 h / Reflux; Inert atmosphere

2: triethylamine / tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

3: methanol; sodium methylate / 20 °C / Inert atmosphere

With methanol; oxalyl dichloride; sodium methylate; triethylamine; In tetrahydrofuran; toluene; 3: Zemplen deprotection;
DOI:10.1039/c1ob05573a

Reference yield:

: 49845-69-4
(R)-O-acetylmandeloyl chloride

: 1329602-79-0
N-[(1S,2R)-2-((2R)-2-hydroxy-phenylacetamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

2: methanol; sodium methylate / 20 °C / Inert atmosphere

With methanol; sodium methylate; triethylamine; In tetrahydrofuran; 2: Zemplen deprotection;
DOI:10.1039/c1ob05573a