1-tosyl-2-<1-(1,1-dimethoxy-2-hydroxy)ethyl>-3,4,4-trimethylimidazolidine

Base Information

Chemical Name:1-tosyl-2-<1-(1,1-dimethoxy-2-hydroxy)ethyl>-3,4,4-trimethylimidazolidine
CAS No.:88939-55-3
Molecular Formula:C₁₇H₂₈N₂O₅S
Molecular Weight:372.486
Hs Code.:

Synonyms:1-tosyl-2-<1-(1,1-dimethoxy-2-hydroxy)ethyl>-3,4,4-trimethylimidazolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-tosyl-2-<1-(1,1-dimethoxy-2-hydroxy)ethyl>-3,4,4-trimethylimidazolidine

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Technology Process of 1-tosyl-2-<1-(1,1-dimethoxy-2-hydroxy)ethyl>-3,4,4-trimethylimidazolidine

There total 2 articles about 1-tosyl-2-<1-(1,1-dimethoxy-2-hydroxy)ethyl>-3,4,4-trimethylimidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 88939-56-4
1-tosyl-2-(dimethoxycarbomethoxy)methyl-3,4,4-trimethylimidazolidine

: 88939-55-3
1-tosyl-2-<1-(1,1-dimethoxy-2-hydroxy)ethyl>-3,4,4-trimethylimidazolidine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 0.166667h; Ambient temperature;
DOI:10.1016/S0040-4020(01)90904-4

Reference yield:

: 71254-91-6
1-tosyl-3,4,4-trimethyl-Δ²-imidazolinium iodide

: 88939-55-3
1-tosyl-2-<1-(1,1-dimethoxy-2-hydroxy)ethyl>-3,4,4-trimethylimidazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) diisopropylamine, n-butyllithium / 1.) THF, -78 deg C, 5 min, 2.) THF, -78 deg C, then RT

2: 98 percent / lithium aluminium hydride / tetrahydrofuran / 0.17 h / Ambient temperature

With lithium aluminium tetrahydride; n-butyllithium; diisopropylamine; In tetrahydrofuran;
DOI:10.1016/S0040-4020(01)90904-4