C₂₉H₄₁NO₂

Base Information

• Chemical Name: C₂₉H₄₁NO₂
• CAS No.: 1394965-62-8
• Molecular Formula: C₂₉H₄₁NO₂
• Molecular Weight: 435.65
• Mol file: 1394965-62-8.mol

Synonyms:C₂₉H₄₁NO₂

Chemical Property of C₂₉H₄₁NO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₄₁NO₂

There total 5 articles about C₂₉H₄₁NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H17NO2 (1394965-69-5) + prenyl bromide (870-63-3) → C29H41NO2 (1394965-62-8)

Guidance literature:

With potassium carbonate; In acetone; for 12h; Reflux;

DOI:10.1016/j.bmc.2012.07.025

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) → C29H41NO2 (1394965-62-8)

Guidance literature:

Multi-step reaction with 5 steps

1: potassium carbonate / acetone / 16 h / Reflux

2: tin(II) chloride dihdyrate / ethanol / 0.33 h / Reflux; Inert atmosphere

3: chloroformic acid ethyl ester; triethylamine / chloroform / 0.75 h / 20 - 50 °C

4: N,N-diethylaniline; hydrogen / 6 h / 200 °C

5: potassium carbonate / acetone / 12 h / Reflux

With tin(II) chloride dihdyrate; hydrogen; chloroformic acid ethyl ester; potassium carbonate; triethylamine; N,N-diethylaniline; In ethanol; chloroform; acetone;

DOI:10.1016/j.bmc.2012.07.025

Reference yield:

p-allyloxyaniline (1688-69-3) → C29H41NO2 (1394965-62-8)

Guidance literature:

Multi-step reaction with 3 steps

1: chloroformic acid ethyl ester; triethylamine / chloroform / 0.75 h / 20 - 50 °C

2: N,N-diethylaniline; hydrogen / 6 h / 200 °C

3: potassium carbonate / acetone / 12 h / Reflux

With hydrogen; chloroformic acid ethyl ester; potassium carbonate; triethylamine; N,N-diethylaniline; In chloroform; acetone;

DOI:10.1016/j.bmc.2012.07.025

upstream raw materials:

4-nitro-phenol

1-allyloxy-4-nitrobenzene

p-allyloxyaniline

N-(4-(allyloxy)phenyl)-1-cyclobutanecarboxamide