C₂₃H₂₁FOSi

Base Information

Chemical Name:C₂₃H₂₁FOSi
CAS No.:1432736-90-7
Molecular Formula:C₂₃H₂₁FOSi
Molecular Weight:360.503
Hs Code.:

Synonyms:C₂₃H₂₁FOSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₂₁FOSi

Chemical Property:

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Technology Process of C₂₃H₂₁FOSi

There total 2 articles about C₂₃H₂₁FOSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1432736-74-7
3-fluoro-1-phenylenyne

: 1432736-88-3
C₁₃H₁₄OSi

: 1432736-90-7
C₂₃H₂₁FOSi

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2′-(diphenylphosphino)-N,N′-dimethyl-(1,1′-biphenyl)-2-amine; In toluene; at 100 ℃; for 72h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol401057z

Reference yield:

: 536-74-3
phenylacetylene

: 1432736-90-7
C₂₃H₂₁FOSi

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / 20 °C / Schlenk technique; Inert atmosphere; Cooling with acetone-dry ice

2: tris-(dibenzylideneacetone)dipalladium(0); 2′-(diphenylphosphino)-N,N′-dimethyl-(1,1′-biphenyl)-2-amine / toluene / 72 h / 100 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; triethylamine; 2′-(diphenylphosphino)-N,N′-dimethyl-(1,1′-biphenyl)-2-amine; In toluene; 1: |Sonogashira Cross-Coupling;
DOI:10.1021/ol401057z

Reference yield:

: 1432736-90-7
C₂₃H₂₁FOSi

: 1420771-02-3
C₂₀H₁₃F

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; toluene; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol401057z