5-Nonanone, (2,4-dinitrophenyl)hydrazone

Base Information

Chemical Name:5-Nonanone, (2,4-dinitrophenyl)hydrazone
CAS No.:3657-08-7
Molecular Formula:C₁₅H₂₂N₄O₄
Molecular Weight:322.364
Hs Code.:2928000090
NSC Number:115637
DSSTox Substance ID:DTXSID30957851
Nikkaji Number:J143.301F
Mol file:3657-08-7.mol

Synonyms:NSC115637;DTXSID30957851;ZCYIGAIUDNMPME-UHFFFAOYSA-N;5-Nonanone,4-dinitrophenyl)hydrazone;NSC-115637;5-Nonanone, (2,4-dinitrophenyl)hydrazone;1-(2,4-dinitrophenyl)-2-(nonan-5-ylidene)hydrazine

Suppliers and Price of 5-Nonanone, (2,4-dinitrophenyl)hydrazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 5-Nonanone, (2,4-dinitrophenyl)hydrazone

Chemical Property:

Vapor Pressure:4.81E-08mmHg at 25°C
Boiling Point:443°Cat760mmHg
Flash Point:221.7°C
PSA：116.03000
Density:1.22g/cm³
LogP:5.77070
XLogP3:5.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:8
Exact Mass:322.16410520
Heavy Atom Count:23
Complexity:407

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCCCC(=NNC1=C(C=C(C=C1)[N+](=O)[O-])[N+](=O)[O-])CCCC

Technology Process of 5-Nonanone, (2,4-dinitrophenyl)hydrazone

There total 18 articles about 5-Nonanone, (2,4-dinitrophenyl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 502-56-7
nonanone-5

: 119-26-6
(2,4-dinitro-phenyl)-hydrazine

: 3657-08-7
nonan-5-one-(2,4-dinitro-phenylhydrazone)

Guidance literature:: With phosphonic acid diethyl ester;

Reference yield:

: 34009-04-6
phenyl pentyl sulfone

: 3657-08-7
nonan-5-one-(2,4-dinitro-phenylhydrazone)

Guidance literature:: Multi-step reaction with 5 steps

1: 81 percent / butyl-lithium / hexane; tetrahydrofuran / 1 h / 0 °C

2: 69 percent / butyl-lithium / hexane; tetrahydrofuran / 0 °C

3: 86 percent / di-isobutylaluminum hydride / toluene / 48 h / Heating

4: 85percent m-chloroperbenzoic acid / CH₂Cl₂ / 1.5 h / -23 °C

With n-butyllithium; diisobutylaluminum hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1039/P19860000195

Reference yield:

: 1129-70-0
pentyl phenyl sulfide

: 3657-08-7
nonan-5-one-(2,4-dinitro-phenylhydrazone)

Guidance literature:: Multi-step reaction with 6 steps

1: m-chloroperbenzoic acid

2: 81 percent / butyl-lithium / hexane; tetrahydrofuran / 1 h / 0 °C

3: 69 percent / butyl-lithium / hexane; tetrahydrofuran / 0 °C

4: 86 percent / di-isobutylaluminum hydride / toluene / 48 h / Heating

5: 85percent m-chloroperbenzoic acid / CH₂Cl₂ / 1.5 h / -23 °C

With n-butyllithium; diisobutylaluminum hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1039/P19860000195