C₃₀H₃₈O₅S₂

Base Information

Chemical Name:C₃₀H₃₈O₅S₂
CAS No.:537658-37-0
Molecular Formula:C₃₀H₃₈O₅S₂
Molecular Weight:542.761
Hs Code.:

C<sub>30</sub>H<sub>38</sub>O<sub>5</sub>S<sub>2</sub>

Synonyms:C₃₀H₃₈O₅S₂

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Chemical Property of C₃₀H₃₈O₅S₂

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Technology Process of C₃₀H₃₈O₅S₂

There total 13 articles about C₃₀H₃₈O₅S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 537658-35-8
C₃₁H₄₂O₆S₂

: 537658-37-0
C₃₀H₃₈O₅S₂

Guidance literature:: With potassium hexamethylsilazane; In tetrahydrofuran; at -78 - 0 ℃; for 3h;
DOI:10.1021/ol034218c

Reference yield:

: 100-39-0
benzyl bromide

: 537658-37-0
C₃₀H₃₈O₅S₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: 78 percent / NaH; Bu₄NI / dimethylformamide / 1 h / 0 - 20 °C

2.1: 75 percent / n-BuLi / tetrahydrofuran; hexane / 0 - 20 °C

3.1: O₃ / CH₂Cl₂; methanol / 0.08 h / -78 °C

3.2: 75 percent / Me₂S / CH₂Cl₂; methanol / 14 h / -78 - 20 °C

4.1: 75 percent / MgBr₂; Et₃N / tetrahydrofuran / 2.5 h

5.1: 100 percent / HF / acetonitrile / 24 h / 20 °C

6.1: 63 percent / DMAP; Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

7.1: toluene / 24 h / 200 °C

8.1: K₂CO₃ / CH₂Cl₂; methanol / 14 h / 20 °C

9.1: 80 percent / NaBH₄ / tetrahydrofuran; H₂O / 16 h / 70 °C

10.1: Mg / methanol / 2 h / 80 °C

11.1: 90 percent / KHMDS / tetrahydrofuran / 3 h / -78 - 0 °C

With dmap; sodium tetrahydroborate; n-butyllithium; hydrogen fluoride; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; sodium hydride; potassium carbonate; ozone; magnesium; triethylamine; magnesium bromide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 4.1: modified Horner-Wadsworth-Emmons reaction / 7.1: intramolecular Diels-Alder reaction / 11.1: Dieckman cyclization;
DOI:10.1021/ol034218c

Reference yield:

: C₁₅H₂₀OS₂

: 537658-37-0
C₃₀H₃₈O₅S₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: KHMDS / tetrahydrofuran / 0.5 h / -78 °C

1.2: tetrahydrofuran / 0.75 h / 0 °C

2.1: 63 percent / DMAP; Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

3.1: toluene / 24 h / 200 °C

4.1: K₂CO₃ / CH₂Cl₂; methanol / 14 h / 20 °C

5.1: 80 percent / NaBH₄ / tetrahydrofuran; H₂O / 16 h / 70 °C

6.1: Mg / methanol / 2 h / 80 °C

7.1: 90 percent / KHMDS / tetrahydrofuran / 3 h / -78 - 0 °C

With dmap; sodium tetrahydroborate; potassium hexamethylsilazane; potassium carbonate; magnesium; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; toluene; 3.1: intramolecular Diels-Alder reaction / 7.1: Dieckman cyclization;
DOI:10.1021/ol034218c