Technology Process of C10H11F2NO5S
There total 3 articles about C10H11F2NO5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: aluminum (III) chloride / dichloromethane / 24 h / 30 °C / Cooling
2: sodium nitrite / acetone / 6 h / 50 °C
3: sodium tetrahydroborate / tetrahydrofuran; water / 2 h / 0 - 20 °C
4: triethylamine / toluene / 2 h / -15 °C
With
aluminum (III) chloride; sodium tetrahydroborate; triethylamine; sodium nitrite;
In
tetrahydrofuran; dichloromethane; water; acetone; toluene;
1: |Friedel-Crafts Acylation;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium nitrite / acetone / 6 h / 50 °C
2: sodium tetrahydroborate / tetrahydrofuran; water / 2 h / 0 - 20 °C
3: triethylamine / toluene / 2 h / -15 °C
With
sodium tetrahydroborate; triethylamine; sodium nitrite;
In
tetrahydrofuran; water; acetone; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium tetrahydroborate / tetrahydrofuran; water / 2 h / 0 - 20 °C
2: triethylamine / toluene / 2 h / -15 °C
With
sodium tetrahydroborate; triethylamine;
In
tetrahydrofuran; water; toluene;