Technology Process of C25H26N4O6S2
There total 6 articles about C25H26N4O6S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
caesium carbonate;
In
acetonitrile;
at 60 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: hydrogenchloride; sodium nitrite / ethanol; water / 0.33 h / 0 °C
1.2: 2 h / 0 °C
2.1: ammonium acetate; acetic acid / 0.75 h / 120 °C / Microwave irradiation
3.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 16 h / 20 °C
3.2: pH 6
4.1: N-ethyl-N,N-diisopropylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / dimethyl sulfoxide / 16 h / 20 °C
5.1: methanesulfonic acid; L-methionine / 72 h
6.1: caesium carbonate / acetonitrile / 16 h / 60 °C
With
hydrogenchloride; methanesulfonic acid; lithium hydroxide monohydrate; L-methionine; ammonium acetate; water; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; sodium nitrite;
In
tetrahydrofuran; ethanol; water; dimethyl sulfoxide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-ethyl-N,N-diisopropylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / dimethyl sulfoxide / 16 h / 20 °C
2: methanesulfonic acid; L-methionine / 72 h
3: caesium carbonate / acetonitrile / 16 h / 60 °C
With
methanesulfonic acid; L-methionine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; N-ethyl-N,N-diisopropylamine;
In
dimethyl sulfoxide; acetonitrile;