3-(2-chloroethyl)-2-oxo-2-benzylamino-1-benzyl-1,3,2λ⁵-diazaphospholidine

Base Information

Chemical Name:3-(2-chloroethyl)-2-oxo-2-benzylamino-1-benzyl-1,3,2λ⁵-diazaphospholidine
CAS No.:256496-41-0
Molecular Formula:C₁₈H₂₃ClN₃OP
Molecular Weight:363.827
Hs Code.:

3-(2-chloroethyl)-2-oxo-2-benzylamino-1-benzyl-1,3,2λ<sup>5</sup>-diazaphospholidine

Synonyms:3-(2-chloroethyl)-2-oxo-2-benzylamino-1-benzyl-1,3,2λ⁵-diazaphospholidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2-chloroethyl)-2-oxo-2-benzylamino-1-benzyl-1,3,2λ⁵-diazaphospholidine

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Technology Process of 3-(2-chloroethyl)-2-oxo-2-benzylamino-1-benzyl-1,3,2λ⁵-diazaphospholidine

There total 2 articles about 3-(2-chloroethyl)-2-oxo-2-benzylamino-1-benzyl-1,3,2λ⁵-diazaphospholidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 256496-40-9
N,N-bis(2-chloroethyl)-N',N-dibenzylphosphoric triamide

: 256496-41-0
3-(2-chloroethyl)-2-oxo-2-benzylamino-1-benzyl-1,3,2λ⁵-diazaphospholidine

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 48h;
DOI:10.1039/a903835c

Reference yield:

: 100-46-9
benzylamine

: 256496-41-0
3-(2-chloroethyl)-2-oxo-2-benzylamino-1-benzyl-1,3,2λ⁵-diazaphospholidine

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / diethyl ether / 142 h / -70 - 20 °C

2: 63 percent / t-BuOK / tetrahydrofuran / 48 h / 20 °C

With potassium tert-butylate; In tetrahydrofuran; diethyl ether; 1: Substitution / 2: Cyclization;
DOI:10.1039/a903835c