benzyl 2-acetamido-3-O-benzyl-4-methoxyimino-2,4,6-trideoxy-α-L-idopyranoside

Base Information

Chemical Name:benzyl 2-acetamido-3-O-benzyl-4-methoxyimino-2,4,6-trideoxy-α-L-idopyranoside
CAS No.:1264439-12-4
Molecular Formula:C₂₃H₂₈N₂O₅
Molecular Weight:412.486
Hs Code.:

Synonyms:benzyl 2-acetamido-3-O-benzyl-4-methoxyimino-2,4,6-trideoxy-α-L-idopyranoside

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Chemical Property of benzyl 2-acetamido-3-O-benzyl-4-methoxyimino-2,4,6-trideoxy-α-L-idopyranoside

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Technology Process of benzyl 2-acetamido-3-O-benzyl-4-methoxyimino-2,4,6-trideoxy-α-L-idopyranoside

There total 7 articles about benzyl 2-acetamido-3-O-benzyl-4-methoxyimino-2,4,6-trideoxy-α-L-idopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1264439-08-8
benzyl 2-acetamido-3-O-benzyl-2,6-dideoxy-4-oxo-α-L-idopyranoside

: 593-56-6
N-methoxylamine hydrochloride

: benzyl 2-acetamido-3-O-benzyl-4-methoxyimino-2,4,6-trideoxy-α-L-idopyranoside

: 1264439-12-4
benzyl 2-acetamido-3-O-benzyl-4-methoxyimino-2,4,6-trideoxy-α-L-idopyranoside

Guidance literature:: With sodium hydrogencarbonate; In methanol; at 65 ℃; for 17h; optical yield given as %de;
DOI:10.1016/j.tetlet.2010.11.078

Reference yield:

: 1264439-47-5
C₃₁H₄₅NO₅Si

: benzyl 2-acetamido-3-O-benzyl-4-methoxyimino-2,4,6-trideoxy-α-L-idopyranoside

: 1264439-12-4
benzyl 2-acetamido-3-O-benzyl-4-methoxyimino-2,4,6-trideoxy-α-L-idopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C

2: Wilkinson's catalyst; hydrogen / ethanol; benzene / 3 h / 20 °C / 760.05 Torr

3: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 17 h / 20 °C

4: sodium hydrogencarbonate / methanol / 17 h / 65 °C

With Wilkinson's catalyst; tetrabutyl ammonium fluoride; hydrogen; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; methanol; ethanol; dichloromethane; benzene;
DOI:10.1016/j.tetlet.2010.11.078

Reference yield:

: 1264439-05-5
benzyl 2-acetamido-3-O-benzyl-2,6-dideoxy-5,6-α-L-idopyranoside

: benzyl 2-acetamido-3-O-benzyl-4-methoxyimino-2,4,6-trideoxy-α-L-idopyranoside

: 1264439-12-4
benzyl 2-acetamido-3-O-benzyl-4-methoxyimino-2,4,6-trideoxy-α-L-idopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 17 h / 20 °C

2: sodium hydrogencarbonate / methanol / 17 h / 65 °C

With sodium hydrogencarbonate; Dess-Martin periodane; In methanol; dichloromethane;
DOI:10.1016/j.tetlet.2010.11.078