2-[2-(1-amino-ethyl)-4-oxo-4H-quinazolin-3-yl]-benzoic acid methyl ester

Base Information

Chemical Name:2-[2-(1-amino-ethyl)-4-oxo-4H-quinazolin-3-yl]-benzoic acid methyl ester
CAS No.:1026949-89-2
Molecular Formula:C₁₈H₁₇N₃O₃
Molecular Weight:323.351
Hs Code.:

2-[2-(1-amino-ethyl)-4-oxo-4<i>H</i>-quinazolin-3-yl]-benzoic acid methyl ester

Synonyms:2-[2-(1-amino-ethyl)-4-oxo-4H-quinazolin-3-yl]-benzoic acid methyl ester

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Chemical Property of 2-[2-(1-amino-ethyl)-4-oxo-4H-quinazolin-3-yl]-benzoic acid methyl ester

Chemical Property:

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Technology Process of 2-[2-(1-amino-ethyl)-4-oxo-4H-quinazolin-3-yl]-benzoic acid methyl ester

There total 4 articles about 2-[2-(1-amino-ethyl)-4-oxo-4H-quinazolin-3-yl]-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-[2-(1-azido-ethyl)-4-oxo-4H-quinazolin-3-yl]-benzoic acid methyl ester

: 1026949-89-2
2-[2-(1-amino-ethyl)-4-oxo-4H-quinazolin-3-yl]-benzoic acid methyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 20 ℃; for 7h; under 11377.3 Torr;
DOI:10.1002/jhet.5570390218

Reference yield:

: 2916-09-8
2-ethyl-benzo[d][1,3]oxazin-4-one

: 1026949-89-2
2-[2-(1-amino-ethyl)-4-oxo-4H-quinazolin-3-yl]-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 5 percent / acetic acid / 3 h / Heating

2: 87 percent / bromine; NaOAc / acetic acid / 1.5 h / 60 °C

3: aq. sodium azide / propan-2-ol / Heating

4: hydrogen / 5 percent Pd/C / ethanol / 7 h / 20 °C / 11377.3 Torr

With sodium azide; hydrogen; bromine; sodium acetate; palladium on activated charcoal; In ethanol; acetic acid; isopropyl alcohol;
DOI:10.1002/jhet.5570390218

Reference yield:

: 94209-49-1
2-(2-ethyl-4-oxo-4H-quinazolin-3-yl)-benzoic acid methyl ester

: 1026949-89-2
2-[2-(1-amino-ethyl)-4-oxo-4H-quinazolin-3-yl]-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / bromine; NaOAc / acetic acid / 1.5 h / 60 °C

2: aq. sodium azide / propan-2-ol / Heating

3: hydrogen / 5 percent Pd/C / ethanol / 7 h / 20 °C / 11377.3 Torr

With sodium azide; hydrogen; bromine; sodium acetate; palladium on activated charcoal; In ethanol; acetic acid; isopropyl alcohol;
DOI:10.1002/jhet.5570390218