2-(6-(4-methoxystyryl)-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N,N-dimethylethanamine

Base Information

Chemical Name:2-(6-(4-methoxystyryl)-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N,N-dimethylethanamine
CAS No.:1283604-03-4
Molecular Formula:C₂₅H₂₄N₂O₃
Molecular Weight:400.477
Hs Code.:

Synonyms:2-(6-(4-methoxystyryl)-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N,N-dimethylethanamine

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Chemical Property of 2-(6-(4-methoxystyryl)-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N,N-dimethylethanamine

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Technology Process of 2-(6-(4-methoxystyryl)-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N,N-dimethylethanamine

There total 2 articles about 2-(6-(4-methoxystyryl)-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N,N-dimethylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 182344-65-6
2-(6-bromo-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N,N-dimethylethanamine

: 637-69-4,24936-44-5
4-Methoxystyrene

: 1283604-03-4
2-(6-(4-methoxystyryl)-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N,N-dimethylethanamine

Guidance literature:: With palladium diacetate; triethylamine; tris-(o-tolyl)phosphine; In acetonitrile; at 105 ℃; for 48h; Sealed bottle; Inert atmosphere;
DOI:10.1039/c0jm02942d

Reference yield:

: 81-86-7
4-bromo-1,8-naphthalenedicarboxylic anhydride

: 1283604-03-4
2-(6-(4-methoxystyryl)-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N,N-dimethylethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 12 h / 20 °C

2: tris-(o-tolyl)phosphine; triethylamine; palladium diacetate / acetonitrile / 48 h / 105 °C / Inert atmosphere; Sealed tube

With palladium diacetate; triethylamine; tris-(o-tolyl)phosphine; In ethanol; acetonitrile; 2: |Heck Reaction;
DOI:10.1039/c7ob02037f