(2R,4'S)-N'-Benzyl-2-<oxy>-1-(4'-oxazolidinyl)-4-pentene

Base Information

Chemical Name:(2R,4'S)-N'-Benzyl-2-<oxy>-1-(4'-oxazolidinyl)-4-pentene
CAS No.:171523-94-7
Molecular Formula:C₂₁H₃₅NO₂Si
Molecular Weight:361.6
Hs Code.:

(2R,4'S)-N'-Benzyl-2-<<dimethyl(2-methyl-2-propyl)silyl>oxy>-1-(4'-oxazolidinyl)-4-pentene

Synonyms:(2R,4'S)-N'-Benzyl-2-<oxy>-1-(4'-oxazolidinyl)-4-pentene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,4'S)-N'-Benzyl-2-<oxy>-1-(4'-oxazolidinyl)-4-pentene

Chemical Property:

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Technology Process of (2R,4'S)-N'-Benzyl-2-<oxy>-1-(4'-oxazolidinyl)-4-pentene

There total 6 articles about (2R,4'S)-N'-Benzyl-2-<oxy>-1-(4'-oxazolidinyl)-4-pentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 171523-93-6
(2S,4R)-2-(N-Benzylamino)-4-<oxy>-6-hepten-1-ol

: 171523-94-7
(2R,4'S)-N'-Benzyl-2-<oxy>-1-(4'-oxazolidinyl)-4-pentene

Guidance literature:: In water; benzene; for 0.5h; Heating;
DOI:10.1021/jo00129a019

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 171523-94-7
(2R,4'S)-N'-Benzyl-2-<oxy>-1-(4'-oxazolidinyl)-4-pentene

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / NEt₃ / CH₂Cl₂ / 0.08 h / 0 °C

2: 92 percent / i-Bu₂AlH / toluene; hexane / 0.08 h / 0 °C

3: 100 percent / benzene; H₂O / 0.5 h / Heating

With diisobutylaluminium hydride; triethylamine; In hexane; dichloromethane; water; toluene; benzene;
DOI:10.1021/jo00129a019

Reference yield:

: 102614-19-7
(4S)-4-(2'-Oxoethyl)-2-phenyloxazoline

: 171523-94-7
(2R,4'S)-N'-Benzyl-2-<oxy>-1-(4'-oxazolidinyl)-4-pentene

Guidance literature:: Multi-step reaction with 4 steps

1: ZnCl₂ / tetrahydrofuran; diethyl ether / 1.) 0 deg C to r.t., 5 min, 2.) 3 h

2: 100 percent / NEt₃ / CH₂Cl₂ / 0.08 h / 0 °C

3: 92 percent / i-Bu₂AlH / toluene; hexane / 0.08 h / 0 °C

4: 100 percent / benzene; H₂O / 0.5 h / Heating

With diisobutylaluminium hydride; triethylamine; zinc(II) chloride; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; toluene; benzene;
DOI:10.1021/jo00129a019