ethyl 6-(2-(1H-imidazol-1-yl)-1-{[(4-methoxyphenyl)methoxy]methyl}ethoxy)-2(E)-hexenoate

Base Information

Chemical Name:ethyl 6-(2-(1H-imidazol-1-yl)-1-{[(4-methoxyphenyl)methoxy]methyl}ethoxy)-2(E)-hexenoate
CAS No.:109786-93-8
Molecular Formula:C₂₂H₃₀N₂O₅
Molecular Weight:402.491
Hs Code.:

Synonyms:ethyl 6-(2-(1H-imidazol-1-yl)-1-{[(4-methoxyphenyl)methoxy]methyl}ethoxy)-2(E)-hexenoate

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Chemical Property of ethyl 6-(2-(1H-imidazol-1-yl)-1-{[(4-methoxyphenyl)methoxy]methyl}ethoxy)-2(E)-hexenoate

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Technology Process of ethyl 6-(2-(1H-imidazol-1-yl)-1-{[(4-methoxyphenyl)methoxy]methyl}ethoxy)-2(E)-hexenoate

There total 3 articles about ethyl 6-(2-(1H-imidazol-1-yl)-1-{[(4-methoxyphenyl)methoxy]methyl}ethoxy)-2(E)-hexenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 109786-92-7
4-<2-(1H-imidazol-1-yl)-1-<<(4-methoxyphenyl)methoxy>methyl>ethoxy>butanal

: 1099-45-2
ethyl (triphenylphosphoranylidene)acetate

: 109786-93-8
ethyl 6-(2-(1H-imidazol-1-yl)-1-{[(4-methoxyphenyl)methoxy]methyl}ethoxy)-2(E)-hexenoate

Guidance literature:: In benzene; for 1h;
DOI:10.1021/jm00393a022

Reference yield:

: 84727-35-5
1-[2-hydroxy-3-[(4-methoxyphenyl)methoxy]propyl]-1H-imidazole

: 109786-93-8
ethyl 6-(2-(1H-imidazol-1-yl)-1-{[(4-methoxyphenyl)methoxy]methyl}ethoxy)-2(E)-hexenoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMSO, 18 deg C, 5 min, 2.) DMSO, 16 h

2: 0.5 M H₂SO₄ / 0.42 h

3: 39 percent / benzene / 1 h

With sulfuric acid; sodium hydride; In benzene;
DOI:10.1021/jm00393a022

Reference yield:

: 109786-91-6
4-<2-(1H-imidazol-1-yl)-1-<<(4-methoxyphenyl)methoxy>methyl>ethoxy>butanal ethylene acetal

: 109786-93-8
ethyl 6-(2-(1H-imidazol-1-yl)-1-{[(4-methoxyphenyl)methoxy]methyl}ethoxy)-2(E)-hexenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 0.5 M H₂SO₄ / 0.42 h

2: 39 percent / benzene / 1 h

With sulfuric acid; In benzene;
DOI:10.1021/jm00393a022