N-(4-bromo-benzyl)-3-cyclopentyl-N-(2-dimethylamino-ethyl)-propionamide

Base Information

Chemical Name:N-(4-bromo-benzyl)-3-cyclopentyl-N-(2-dimethylamino-ethyl)-propionamide
CAS No.:864741-96-8
Molecular Formula:C₁₉H₂₉BrN₂O
Molecular Weight:381.356
Hs Code.:

<i>N</i>-(4-bromo-benzyl)-3-cyclopentyl-<i>N</i>-(2-dimethylamino-ethyl)-propionamide

Synonyms:N-(4-bromo-benzyl)-3-cyclopentyl-N-(2-dimethylamino-ethyl)-propionamide

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Chemical Property of N-(4-bromo-benzyl)-3-cyclopentyl-N-(2-dimethylamino-ethyl)-propionamide

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Technology Process of N-(4-bromo-benzyl)-3-cyclopentyl-N-(2-dimethylamino-ethyl)-propionamide

There total 2 articles about N-(4-bromo-benzyl)-3-cyclopentyl-N-(2-dimethylamino-ethyl)-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 104-97-2
cyclopentanepropanoyl chloride

: 99862-34-7
N'-(4-bromobenzyl)-N,N-dimethylethane-1,2-diamine

: 864741-96-8
N-(4-bromo-benzyl)-3-cyclopentyl-N-(2-dimethylamino-ethyl)-propionamide

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1016/j.bmcl.2005.06.024

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 864741-96-8
N-(4-bromo-benzyl)-3-cyclopentyl-N-(2-dimethylamino-ethyl)-propionamide

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / NaBH(OAc)3; AcOH / CH₂Cl₂

2: 100 percent / Et₃N / CH₂Cl₂

With sodium tris(acetoxy)borohydride; acetic acid; triethylamine; In dichloromethane;
DOI:10.1016/j.bmcl.2005.06.024

Reference yield:

: 864741-96-8
N-(4-bromo-benzyl)-3-cyclopentyl-N-(2-dimethylamino-ethyl)-propionamide

: SB 699551

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / Pd(PPh₃)4; Na₂CO₃ / H₂O; 1,2-dimethoxy-ethane

2: 57 percent / NaBH(OAc)3; AcOH / CH₂Cl₂

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium tris(acetoxy)borohydride; sodium carbonate; acetic acid; In 1,2-dimethoxyethane; dichloromethane; water;
DOI:10.1016/j.bmcl.2005.06.024