2-[(bromoacetyl)(2-phenylethyl)amino]ethyl carbamic acid tert-butyl ester

Base Information

Chemical Name:2-[(bromoacetyl)(2-phenylethyl)amino]ethyl carbamic acid tert-butyl ester
CAS No.:190953-68-5
Molecular Formula:C₁₇H₂₅BrN₂O₃
Molecular Weight:385.301
Hs Code.:

Synonyms:2-[(bromoacetyl)(2-phenylethyl)amino]ethyl carbamic acid tert-butyl ester

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Chemical Property of 2-[(bromoacetyl)(2-phenylethyl)amino]ethyl carbamic acid tert-butyl ester

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Technology Process of 2-[(bromoacetyl)(2-phenylethyl)amino]ethyl carbamic acid tert-butyl ester

There total 4 articles about 2-[(bromoacetyl)(2-phenylethyl)amino]ethyl carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 598-21-0
2-Bromoacetyl bromide

: 190953-67-4
2-(2-phenylethylamino)ethylcarbamic acid tert-butyl ester

: 190953-68-5
2-[(bromoacetyl)(2-phenylethyl)amino]ethyl carbamic acid tert-butyl ester

Guidance literature:: With triethylamine; In dichloromethane; at -10 ℃; for 0.5h;
DOI:10.1021/jm980569z

Reference yield: 79.0%

: 190953-68-5
2-[(bromoacetyl)(2-phenylethyl)amino]ethyl carbamic acid tert-butyl ester

Guidance literature:

Reference yield:

: 39684-80-5
2-(tert-butoxycarbonylamino)ethyl bromide

: 190953-68-5
2-[(bromoacetyl)(2-phenylethyl)amino]ethyl carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / K₂CO₃ / dimethylformamide / 4 h / 60 °C

2: 79 percent / Et₃N / CH₂Cl₂ / 0.5 h / -10 °C

With potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm980569z