C₁₃H₁₂BrNO₃

Base Information

Chemical Name:C₁₃H₁₂BrNO₃
CAS No.:1072297-45-0
Molecular Formula:C₁₃H₁₂BrNO₃
Molecular Weight:310.147
Hs Code.:

C<sub>13</sub>H<sub>12</sub>BrNO<sub>3</sub>

Synonyms:C₁₃H₁₂BrNO₃

Suppliers and Price of C₁₃H₁₂BrNO₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₃H₁₂BrNO₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₃H₁₂BrNO₃

There total 4 articles about C₁₃H₁₂BrNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1072297-44-9
C₁₁H₈BrNO₃

: 1119-22-8
divinyl zinc

: 1072297-45-0
C₁₃H₁₂BrNO₃

Guidance literature:: divinyl zinc; With (1S,2R)-2-(morpholin-4-yl)-1-phenylpropanol; n-butyllithium; In tetrahydrofuran; 1,4-dioxane; hexanes; diethyl ether; toluene; at 0 ℃; for 1h;

C₁₁H₈BrNO₃; In tetrahydrofuran; 1,4-dioxane; hexanes; diethyl ether; toluene; at -75 - -30 ℃; for 1h;

With water; citric acid; In tetrahydrofuran; 1,4-dioxane; hexanes; diethyl ether; toluene; at -30 - 23 ℃;

Reference yield:

: 123320-44-5
(3-(benzyloxy)isoxazol-5-yl)methanol

: 1072297-45-0
C₁₃H₁₂BrNO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: bromine / tetrahydrofuran / 6 h / 0 °C

2.1: 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium hydrogencarbonate; potassium bromide / dichloromethane; water / 0.25 h / 23 °C

3.1: (1S,2R)-2-(morpholin-4-yl)-1-phenylpropanol; n-butyllithium / tetrahydrofuran; 1,4-dioxane; hexanes; diethyl ether; toluene / 1 h / 0 °C

3.2: 1 h / -75 - -30 °C

3.3: -30 - 23 °C

With (1S,2R)-2-(morpholin-4-yl)-1-phenylpropanol; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; n-butyllithium; bromine; sodium hydrogencarbonate; potassium bromide; In tetrahydrofuran; 1,4-dioxane; hexanes; diethyl ether; dichloromethane; water; toluene;

Reference yield:

: 205115-22-6
3-benzyloxyisoxazole-5-carboxylic acid methyl ester

: 1072297-45-0
C₁₃H₁₂BrNO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanol; sodium tetrahydroborate

2.1: bromine / tetrahydrofuran / 6 h / 0 °C

3.1: 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium hydrogencarbonate; potassium bromide / dichloromethane; water / 0.25 h / 23 °C

4.1: (1S,2R)-2-(morpholin-4-yl)-1-phenylpropanol; n-butyllithium / tetrahydrofuran; 1,4-dioxane; hexanes; diethyl ether; toluene / 1 h / 0 °C

4.2: 1 h / -75 - -30 °C

4.3: -30 - 23 °C

With methanol; (1S,2R)-2-(morpholin-4-yl)-1-phenylpropanol; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium tetrahydroborate; n-butyllithium; bromine; sodium hydrogencarbonate; potassium bromide; In tetrahydrofuran; 1,4-dioxane; hexanes; diethyl ether; dichloromethane; water; toluene;