4-tolyl 4,6-O-benzylidine-3-O-chloroacetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:4-tolyl 4,6-O-benzylidine-3-O-chloroacetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside
CAS No.:1347109-79-8
Molecular Formula:C₃₀H₂₆ClNO₇S
Molecular Weight:580.058
Hs Code.:

Synonyms:4-tolyl 4,6-O-benzylidine-3-O-chloroacetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

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Chemical Property of 4-tolyl 4,6-O-benzylidine-3-O-chloroacetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

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Technology Process of 4-tolyl 4,6-O-benzylidine-3-O-chloroacetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

There total 2 articles about 4-tolyl 4,6-O-benzylidine-3-O-chloroacetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 541-88-8
Chloroacetic anhydride

: 220645-16-9
4-methylphenyl 4,6-O-benzylidene-2-deoxyl-1-thio-2-phthalimido-β-D-glucopyranoside

: 1347109-79-8
4-tolyl 4,6-O-benzylidine-3-O-chloroacetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: With pyridine; In dichloromethane; at -5 ℃; for 0.75h;
DOI:10.1055/s-0034-1380922

Reference yield:

: 79-04-9
chloroacetyl chloride

: 220645-16-9
4-methylphenyl 4,6-O-benzylidene-2-deoxyl-1-thio-2-phthalimido-β-D-glucopyranoside

: 1347109-79-8
4-tolyl 4,6-O-benzylidine-3-O-chloroacetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/ol201806d

Reference yield: 87.0%

: 1347109-79-8
4-tolyl 4,6-O-benzylidine-3-O-chloroacetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 4-methoxyphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1→2)-3,6-di-O-benzyl-β-D-glucopyranoside

: 4-methoxyphenyl 4,6-O-benzylidine-3-O-chloroacetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-(2,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; sulfuric acid; silica gel; In dichloromethane; at 0 ℃; for 0.0833333h; Molecular sieve; Inert atmosphere;
DOI:10.1055/s-0034-1380922