2-benzyl-2-[2,6-bis(dibenzylamino)-5-nitropyrimidin-4-yl]-3-phenylpropionitrile

Base Information

Chemical Name:2-benzyl-2-[2,6-bis(dibenzylamino)-5-nitropyrimidin-4-yl]-3-phenylpropionitrile
CAS No.:724762-15-6
Molecular Formula:C₄₈H₄₂N₆O₂
Molecular Weight:734.9
Hs Code.:

Synonyms:2-benzyl-2-[2,6-bis(dibenzylamino)-5-nitropyrimidin-4-yl]-3-phenylpropionitrile

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Chemical Property of 2-benzyl-2-[2,6-bis(dibenzylamino)-5-nitropyrimidin-4-yl]-3-phenylpropionitrile

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Technology Process of 2-benzyl-2-[2,6-bis(dibenzylamino)-5-nitropyrimidin-4-yl]-3-phenylpropionitrile

There total 7 articles about 2-benzyl-2-[2,6-bis(dibenzylamino)-5-nitropyrimidin-4-yl]-3-phenylpropionitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 724762-14-5
2-[2,6-bis(benzylamino)-5-nitropyridin-4-yl]-3-phenylpropionitrile

: 100-39-0
benzyl bromide

: 724762-15-6
2-benzyl-2-[2,6-bis(dibenzylamino)-5-nitropyrimidin-4-yl]-3-phenylpropionitrile

Guidance literature:: With sodium hydride; In dimethyl sulfoxide;
DOI:10.1016/j.bmc.2004.04.003

Reference yield:

: 724762-11-2
N²,N⁴-dibenzyl-6-bromomethyl-5-nitropyrimidine-2,4-diamine

: 724762-15-6
2-benzyl-2-[2,6-bis(dibenzylamino)-5-nitropyrimidin-4-yl]-3-phenylpropionitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / dimethylsulfoxide / 0.33 h / 20 °C

2: 71 percent / tributylamine / dimethylsulfoxide

3: 82 percent / NaH / dimethylsulfoxide

With tributyl-amine; sodium hydride; In dimethyl sulfoxide;
DOI:10.1016/j.bmc.2004.04.003

Reference yield:

: 724762-13-4
[2,6-bis(benzylamino)-5-nitropyridin-4-yl]acetonitrile

: 724762-15-6
2-benzyl-2-[2,6-bis(dibenzylamino)-5-nitropyrimidin-4-yl]-3-phenylpropionitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / tributylamine / dimethylsulfoxide

2: 82 percent / NaH / dimethylsulfoxide

With tributyl-amine; sodium hydride; In dimethyl sulfoxide;
DOI:10.1016/j.bmc.2004.04.003