methyl 2-acetamido-2,6-dideoxy-3-O-(p-methoxybenzyl)4-O-methylsulfonyl-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2-acetamido-2,6-dideoxy-3-O-(p-methoxybenzyl)4-O-methylsulfonyl-α-D-glucopyranoside
CAS No.:93414-78-9
Molecular Formula:C₁₈H₂₇NO₈S
Molecular Weight:417.48
Hs Code.:

Synonyms:methyl 2-acetamido-2,6-dideoxy-3-O-(p-methoxybenzyl)4-O-methylsulfonyl-α-D-glucopyranoside

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Chemical Property of methyl 2-acetamido-2,6-dideoxy-3-O-(p-methoxybenzyl)4-O-methylsulfonyl-α-D-glucopyranoside

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Technology Process of methyl 2-acetamido-2,6-dideoxy-3-O-(p-methoxybenzyl)4-O-methylsulfonyl-α-D-glucopyranoside

There total 5 articles about methyl 2-acetamido-2,6-dideoxy-3-O-(p-methoxybenzyl)4-O-methylsulfonyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 93414-77-8
methyl 2-acetamido-2-deoxy-3-O-(p-methoxybenzyl)-4,6-di-O-methylsulfonyl-α-D-glucopyranoside

: 93414-78-9
methyl 2-acetamido-2,6-dideoxy-3-O-(p-methoxybenzyl)4-O-methylsulfonyl-α-D-glucopyranoside

Guidance literature:: With sodium tetrahydroborate; dimethyl sulfoxide; In acetic acid; at 5 ℃;
DOI:10.1016/0008-6215(84)85062-4

Reference yield:

: 2746-25-0
p-Methoxybenzyl bromide

: 93414-78-9
methyl 2-acetamido-2,6-dideoxy-3-O-(p-methoxybenzyl)4-O-methylsulfonyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 69 percent / sodium hydride / dimethylformamide / 1 h / 0 °C

2: aq. acetic acid / 0.17 h / 85 °C

3: pyridine / 2 h / Ambient temperature

4: 65 percent / sodium borohydride, methyl sulfoxide / aq. acetic acid / 5 °C

With sodium tetrahydroborate; sodium hydride; acetic acid; dimethyl sulfoxide; In pyridine; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(84)85062-4

Reference yield:

: 139760-20-6
Methyl 2-acetamido-2-deoxy-3-O-(p-methoxybenzyl)-α-D-glucopyranoside

: 93414-78-9
methyl 2-acetamido-2,6-dideoxy-3-O-(p-methoxybenzyl)4-O-methylsulfonyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 2 h / Ambient temperature

2: 65 percent / sodium borohydride, methyl sulfoxide / aq. acetic acid / 5 °C

With sodium tetrahydroborate; dimethyl sulfoxide; In pyridine; acetic acid;
DOI:10.1016/0008-6215(84)85062-4