methyl 2-acetamido-4-azido-2,4,6-trideoxy-3-O-(p-methoxybenzyl)-α-D-galactopyranoside

Base Information

Chemical Name:methyl 2-acetamido-4-azido-2,4,6-trideoxy-3-O-(p-methoxybenzyl)-α-D-galactopyranoside
CAS No.:93414-79-0
Molecular Formula:C₁₇H₂₄N₄O₅
Molecular Weight:364.401
Hs Code.:

Synonyms:methyl 2-acetamido-4-azido-2,4,6-trideoxy-3-O-(p-methoxybenzyl)-α-D-galactopyranoside

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Chemical Property of methyl 2-acetamido-4-azido-2,4,6-trideoxy-3-O-(p-methoxybenzyl)-α-D-galactopyranoside

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Technology Process of methyl 2-acetamido-4-azido-2,4,6-trideoxy-3-O-(p-methoxybenzyl)-α-D-galactopyranoside

There total 6 articles about methyl 2-acetamido-4-azido-2,4,6-trideoxy-3-O-(p-methoxybenzyl)-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 93414-78-9
methyl 2-acetamido-2,6-dideoxy-3-O-(p-methoxybenzyl)4-O-methylsulfonyl-α-D-glucopyranoside

: 93414-79-0
methyl 2-acetamido-4-azido-2,4,6-trideoxy-3-O-(p-methoxybenzyl)-α-D-galactopyranoside

Guidance literature:: With sodium azide; In various solvent(s); at 125 ℃; for 20h;
DOI:10.1016/0008-6215(84)85062-4

Reference yield:

: 2746-25-0
p-Methoxybenzyl bromide

: 93414-79-0
methyl 2-acetamido-4-azido-2,4,6-trideoxy-3-O-(p-methoxybenzyl)-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 69 percent / sodium hydride / dimethylformamide / 1 h / 0 °C

2: aq. acetic acid / 0.17 h / 85 °C

3: pyridine / 2 h / Ambient temperature

4: 65 percent / sodium borohydride, methyl sulfoxide / aq. acetic acid / 5 °C

5: 76 percent / sodium azide / various solvent(s) / 20 h / 125 °C

With sodium tetrahydroborate; sodium azide; sodium hydride; acetic acid; dimethyl sulfoxide; In pyridine; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(84)85062-4

Reference yield:

: 139760-20-6
Methyl 2-acetamido-2-deoxy-3-O-(p-methoxybenzyl)-α-D-glucopyranoside

: 93414-79-0
methyl 2-acetamido-4-azido-2,4,6-trideoxy-3-O-(p-methoxybenzyl)-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 2 h / Ambient temperature

2: 65 percent / sodium borohydride, methyl sulfoxide / aq. acetic acid / 5 °C

3: 76 percent / sodium azide / various solvent(s) / 20 h / 125 °C

With sodium tetrahydroborate; sodium azide; dimethyl sulfoxide; In pyridine; acetic acid;
DOI:10.1016/0008-6215(84)85062-4