3-(1,3,2-Dioxaborinan-2-yl)-N-ethylbenzenamine

Base Information

Chemical Name:3-(1,3,2-Dioxaborinan-2-yl)-N-ethylbenzenamine
CAS No.:267660-72-0
Molecular Formula:C₁₁H₁₆BNO₂
Molecular Weight:205.065
Hs Code.:
DSSTox Substance ID:DTXSID601248699

Synonyms:DTXSID601248699;3-(1,3,2-Dioxaborinan-2-yl)-N-ethylbenzenamine;267660-72-0

Suppliers and Price of 3-(1,3,2-Dioxaborinan-2-yl)-N-ethylbenzenamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(1,3,2-Dioxaborinan-2-yl)-N-ethylbenzenamine

Chemical Property:

Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:205.1274089
Heavy Atom Count:15
Complexity:185

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:B1(OCCCO1)C2=CC(=CC=C2)NCC

Technology Process of 3-(1,3,2-Dioxaborinan-2-yl)-N-ethylbenzenamine

There total 3 articles about 3-(1,3,2-Dioxaborinan-2-yl)-N-ethylbenzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 267660-71-9
3-(N-Ethylamino)phenylboronic acid

: 504-63-2
trimethyleneglycol

: 267660-72-0
N-Ethyl-3-(1,3,2-dioxaborinan-2-yl)aniline

Guidance literature:: In toluene; for 14h; Heating;
DOI:10.1039/a906708f

Reference yield:

: 78887-39-5
3-Acetamidophenylboronic acid

: 267660-72-0
N-Ethyl-3-(1,3,2-dioxaborinan-2-yl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1: 71.6 percent / BH₃*Me₂S / tetrahydrofuran / 6 h / 60 °C

2: 100 percent / toluene / 14 h / Heating

With dimethylsulfide borane complex; In tetrahydrofuran; toluene; 1: Reduction / 2: Etherification;
DOI:10.1039/a906708f

Reference yield:

: 30418-59-8,280563-63-5
3-Aminophenylboronic acid

: 267660-72-0
N-Ethyl-3-(1,3,2-dioxaborinan-2-yl)aniline

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / 14 h / 20 °C

2: 71.6 percent / BH₃*Me₂S / tetrahydrofuran / 6 h / 60 °C

3: 100 percent / toluene / 14 h / Heating

With dimethylsulfide borane complex; triethylamine; In tetrahydrofuran; toluene; 1: Acylation / 2: Reduction / 3: Etherification;
DOI:10.1039/a906708f