4,4'-Bis{N-[3-(1,3,2-dioxaborinan-2-yl)phenyl]-N-ethylcarbamoyl}-2,2'-bipyridine

Base Information

Chemical Name:4,4'-Bis{N-[3-(1,3,2-dioxaborinan-2-yl)phenyl]-N-ethylcarbamoyl}-2,2'-bipyridine
CAS No.:267660-73-1
Molecular Formula:C₃₄H₃₆B₂N₄O₆
Molecular Weight:618.305
Hs Code.:

Synonyms:4,4'-Bis{N-[3-(1,3,2-dioxaborinan-2-yl)phenyl]-N-ethylcarbamoyl}-2,2'-bipyridine

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Chemical Property of 4,4'-Bis{N-[3-(1,3,2-dioxaborinan-2-yl)phenyl]-N-ethylcarbamoyl}-2,2'-bipyridine

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Technology Process of 4,4'-Bis{N-[3-(1,3,2-dioxaborinan-2-yl)phenyl]-N-ethylcarbamoyl}-2,2'-bipyridine

There total 5 articles about 4,4'-Bis{N-[3-(1,3,2-dioxaborinan-2-yl)phenyl]-N-ethylcarbamoyl}-2,2'-bipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.8%

: 72460-28-7
2,2'-bipyridyl-4,4'-dicarboxylic acid chloride

: 267660-72-0
N-Ethyl-3-(1,3,2-dioxaborinan-2-yl)aniline

: 267660-73-1
4,4'-Bis{N-[3-(1,3,2-dioxaborinan-2-yl)phenyl]-N-ethylcarbamoyl}-2,2'-bipyridine

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 15h;
DOI:10.1039/a906708f

Reference yield:

: 78887-39-5
3-Acetamidophenylboronic acid

: 267660-73-1
4,4'-Bis{N-[3-(1,3,2-dioxaborinan-2-yl)phenyl]-N-ethylcarbamoyl}-2,2'-bipyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 71.6 percent / BH₃*Me₂S / tetrahydrofuran / 6 h / 60 °C

2: 100 percent / toluene / 14 h / Heating

3: 6.8 percent / triethylamine / tetrahydrofuran / 15 h / 20 °C

With dimethylsulfide borane complex; triethylamine; In tetrahydrofuran; toluene; 1: Reduction / 2: Etherification / 3: Acylation;
DOI:10.1039/a906708f

Reference yield:

: 6813-38-3
2,2'-Bipyridine-4,4'-dicarboxylic acid

: 267660-73-1
4,4'-Bis{N-[3-(1,3,2-dioxaborinan-2-yl)phenyl]-N-ethylcarbamoyl}-2,2'-bipyridine

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂

2: 6.8 percent / triethylamine / tetrahydrofuran / 15 h / 20 °C

With thionyl chloride; triethylamine; In tetrahydrofuran; 1: Substitution / 2: Acylation;
DOI:10.1039/a906708f