(R)-5-acetoxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine

Base Information

• Chemical Name: (R)-5-acetoxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine
• CAS No.: 193686-81-6
• Molecular Formula: C₁₉H₂₁NO₄S
• Molecular Weight: 359.446

Synonyms:(R)-5-acetoxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine

Chemical Property of (R)-5-acetoxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine

Chemical Property:

Purity/Quality:

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Technology Process of (R)-5-acetoxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine

There total 3 articles about (R)-5-acetoxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

vinyl acetate (108-05-4,9003-20-7) + 5-hydroxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine (19673-33-7) → (S)-5-hydroxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine (193686-79-2) + (R)-5-acetoxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine (193686-81-6) + (S)-5-acetoxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine

Guidance literature:

With Lipase QL; In hexane; at 40 ℃; for 27h;

DOI:10.1016/S0040-4020(00)00388-4

Reference yield: 25.0%

vinyl acetate (108-05-4,9003-20-7) + 5-hydroxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine (19673-33-7) → (R)-5-hydroxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine (193686-83-8) + (S)-5-hydroxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine (193686-79-2) + (R)-5-acetoxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine (193686-81-6)

Guidance literature:

With Lipase PL; In hexane; at 40 ℃; for 30h;

DOI:10.1016/S0040-4020(00)00388-4

Reference yield:

vinyl acetate (108-05-4,9003-20-7) + (R)-5-hydroxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine (193686-83-8) → (R)-5-acetoxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine (193686-81-6)

Guidance literature:

With Lipase PL; In hexane; at 40 ℃; for 72h;

DOI:10.1016/S0040-4020(00)00388-4

upstream raw materials:

vinyl acetate

5-hydroxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine

(R)-5-hydroxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine

Downstream raw materials:

(R)-5-hydroxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine

(R)-5-methoxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine

5-azido-1-(toluene-4-sulfonyl)-2,3,4,5-tetrahydro-1H-benzo[b]azepine

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