Technology Process of C14H15BrFNO4
There total 7 articles about C14H15BrFNO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C20H29BrFNO4Si;
With
hydrogenchloride;
In
tetrahydrofuran; water;
at 0 ℃;
for 2h;
With
sodium hydrogencarbonate;
In
tetrahydrofuran; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium hydroxide; hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 16 h / 20 °C / pH 9
2.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 16 h / pH 2
2.2: pH 7
3.1: calcium chloride / diethyl ether / 3 h / 20 °C
4.1: titanium(IV) isopropylate / tetrahydrofuran / 0.5 h / 140 °C / Microwave irradiation
4.2: 2 h
5.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 0 °C
With
titanium(IV) isopropylate; hydrogenchloride; potassium hydroxide; hydroxylamine hydrochloride; methyl orange; sodium cyanoborohydride; calcium chloride;
In
tetrahydrofuran; methanol; diethyl ether; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 16 h / pH 2
1.2: pH 7
2.1: calcium chloride / diethyl ether / 3 h / 20 °C
3.1: titanium(IV) isopropylate / tetrahydrofuran / 0.5 h / 140 °C / Microwave irradiation
3.2: 2 h
4.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 0 °C
With
titanium(IV) isopropylate; hydrogenchloride; methyl orange; sodium cyanoborohydride; calcium chloride;
In
tetrahydrofuran; methanol; diethyl ether; water;
