benzyl ((2S)-1-(((2R)-2-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-2-hydroxyethyl)amino)-1-oxopropan-2-yl)carbamate

Base Information

Chemical Name:benzyl ((2S)-1-(((2R)-2-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-2-hydroxyethyl)amino)-1-oxopropan-2-yl)carbamate
CAS No.:1343471-55-5
Molecular Formula:C₂₇H₃₄N₂O₈
Molecular Weight:514.576
Hs Code.:

Synonyms:benzyl ((2S)-1-(((2R)-2-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-2-hydroxyethyl)amino)-1-oxopropan-2-yl)carbamate

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Chemical Property of benzyl ((2S)-1-(((2R)-2-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-2-hydroxyethyl)amino)-1-oxopropan-2-yl)carbamate

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Technology Process of benzyl ((2S)-1-(((2R)-2-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-2-hydroxyethyl)amino)-1-oxopropan-2-yl)carbamate

There total 1 articles about benzyl ((2S)-1-(((2R)-2-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-2-hydroxyethyl)amino)-1-oxopropan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1142-20-7
N-Cbz-Ala

: 5-[2-(amino)propan-2-yl]-3-O-benzyl-1,2-O-isopropylidene-α-D-xylofuranose

: 1343471-55-5
benzyl ((2S)-1-(((2R)-2-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-2-hydroxyethyl)amino)-1-oxopropan-2-yl)carbamate

Guidance literature:: With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In acetonitrile; at 20 ℃; for 12h;
DOI:10.1039/c1ob06215h

Reference yield: 72.0%

: 1343471-55-5
benzyl ((2S)-1-(((2R)-2-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-2-hydroxyethyl)amino)-1-oxopropan-2-yl)carbamate

: 1343471-56-6
benzyl ((2S)-1-((2-((3aR,5S,6S,6aR)-6-benzyloxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-2-oxoethyl)amino)-1-oxopropan-2-yl)carbamate

Guidance literature:: With sodium acetate; pyridinium chlorochromate; In dichloromethane; at 0 - 20 ℃; for 5h; Molecular sieve;
DOI:10.1039/c1ob06215h

Reference yield:

: 1343471-55-5
benzyl ((2S)-1-(((2R)-2-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-2-hydroxyethyl)amino)-1-oxopropan-2-yl)carbamate

: C₁₉H₂₆N₂O₅

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate; pyridinium chlorochromate / dichloromethane / 5 h / 0 - 20 °C / Molecular sieve

2: hydrogen; palladium(II) hydroxide / methanol / 24 h / 6205.94 Torr

With hydrogen; sodium acetate; palladium(II) hydroxide; pyridinium chlorochromate; In methanol; dichloromethane;
DOI:10.1039/c1ob06215h