N₁,N₁'-{3,3'-[2,2'-oxybis(ethane-2,1-diyl)bis(oxy)]bis(propane-3,1-diyl)}bis(3-bromoaniline)

Base Information

• Chemical Name: N₁,N₁'-{3,3'-[2,2'-oxybis(ethane-2,1-diyl)bis(oxy)]bis(propane-3,1-diyl)}bis(3-bromoaniline)
• CAS No.: 1000270-06-3
• Molecular Formula: C₂₂H₃₀Br₂N₂O₃
• Molecular Weight: 530.3

Synonyms:N₁,N₁'-{3,3'-[2,2'-oxybis(ethane-2,1-diyl)bis(oxy)]bis(propane-3,1-diyl)}bis(3-bromoaniline)

Chemical Property of N₁,N₁'-{3,3'-[2,2'-oxybis(ethane-2,1-diyl)bis(oxy)]bis(propane-3,1-diyl)}bis(3-bromoaniline)

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Technology Process of N₁,N₁'-{3,3'-[2,2'-oxybis(ethane-2,1-diyl)bis(oxy)]bis(propane-3,1-diyl)}bis(3-bromoaniline)

There total 2 articles about N₁,N₁'-{3,3'-[2,2'-oxybis(ethane-2,1-diyl)bis(oxy)]bis(propane-3,1-diyl)}bis(3-bromoaniline) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

4,7,10-trioxa-1,13-diaminotridecane (4246-51-9) + 1-Bromo-3-iodobenzene (591-18-4) → N1,N1'-{3,3'-[2,2'-oxybis(ethane-2,1-diyl)bis(oxy)]bis(propane-3,1-diyl)}bis(3-bromoaniline) (1000270-06-3)

Guidance literature:

With copper(l) iodide; 2-(2-methyl-1-oxopropane)cyclohexanone; caesium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 24h; Inert atmosphere;

DOI:10.1002/ejoc.201100483

Reference yield: 29.0%

4,7,10-trioxa-1,13-diaminotridecane (4246-51-9) + 1,3-dibromobenzene (108-36-1) → 3-bromo-N-[3-(2-{2-[3-(phenylamino)propoxy]ethoxy}ethoxy)propyl]benzenamine (1000270-08-5) + N1,N1'-{3,3'-[2,2'-oxybis(ethane-2,1-diyl)bis(oxy)]bis(propane-3,1-diyl)}bis(3-bromoaniline) (1000270-06-3) + N1,N3-bis[3-(2-{2-[3-(3-bromophenylamino)propoxy]ethoxy}ethoxy)propyl]benzene-1,3-diamine (1000270-07-4)

Guidance literature:

1,3-dibromobenzene; With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In 1,4-dioxane; at 20 ℃;

4,7,10-trioxa-1,13-diaminotridecane; With sodium t-butanolate; In 1,4-dioxane; Further stages.; Heating;

DOI:10.1055/s-2007-990779

upstream raw materials:

4,7,10-trioxa-1,13-diaminotridecane

1,3-dibromobenzene

1-Bromo-3-iodobenzene

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