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1-nitroso-2-phenyl-ortho-carborane

Base Information Edit
  • Chemical Name:1-nitroso-2-phenyl-ortho-carborane
  • CAS No.:23939-99-3
  • Molecular Formula:C8H15B10NO
  • Molecular Weight:249.323
  • Hs Code.:
  • Mol file:23939-99-3.mol
1-nitroso-2-phenyl-ortho-carborane

Synonyms:1-nitroso-2-phenyl-ortho-carborane

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Chemical Property of 1-nitroso-2-phenyl-ortho-carborane Edit
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Technology Process of 1-nitroso-2-phenyl-ortho-carborane

There total 3 articles about 1-nitroso-2-phenyl-ortho-carborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In 1,2-dimethoxyethane; diethyl ether; (N2); hexane soln. of n-BuLi added to Et2O/DME soln. of carborane deriv.; lithio-carborane deriv. soln. added dropwise to ClNO soln. at -40°C during 35 min; allowed to reach room temp. during 3 h; added in small portions to aq. KHCO3; organic layer dild. with Et2O; washed with H2O; dried and evapd; residue triturated with MeOH; elem. anal.;
DOI:10.1016/j.poly.2008.12.014
Guidance literature:
1-phenyl-1,2-closo-C2B10H11; With n-butyllithium; In diethyl ether; Inert atmosphere; Schlenk technique;
nitrosylchloride; at -78 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1039/c5dt04831a
Guidance literature:
In diethyl ether; pentane; (N2); hexane soln. of n-BuLi added to Et2O/pentane soln. of carborane deriv.; lithio-carborane deriv. soln. added dropwise to ClNO soln. at -117°C during 35 min; allowed to reach room temp. during 3 h; added in small portions to aq. KHCO3; organic layer dild. with Et2O; washed with H2O; dried and evapd; residue triturated with MeOH; elem. anal.;
DOI:10.1016/j.poly.2008.12.014
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