[C6H5CH2OC5H2N(CH2SC6H4CH2OC5H2N(CH2OC5H2N(COOC2H5)2)2)2]Pd(η3-1,1-dimethylallyl)(CF3SO3)

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Chemical Name:[C6H5CH2OC5H2N(CH2SC6H4CH2OC5H2N(CH2OC5H2N(COOC2H5)2)2)2]Pd(η3-1,1-dimethylallyl)(CF3SO3)
CAS No.:474976-24-4
Molecular Formula:CF₃O₃S*C₉₁H₉₄N₇O₂₃PdS₂
Molecular Weight:1973.4
Hs Code.:

Synonyms:[C6H5CH2OC5H2N(CH2SC6H4CH2OC5H2N(CH2OC5H2N(COOC2H5)2)2)2]Pd(η3-1,1-dimethylallyl)(CF3SO3)

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Chemical Property of [C6H5CH2OC5H2N(CH2SC6H4CH2OC5H2N(CH2OC5H2N(COOC2H5)2)2)2]Pd(η3-1,1-dimethylallyl)(CF3SO3)

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Technology Process of [C6H5CH2OC5H2N(CH2SC6H4CH2OC5H2N(CH2OC5H2N(COOC2H5)2)2)2]Pd(η3-1,1-dimethylallyl)(CF3SO3)

There total 1 articles about [C6H5CH2OC5H2N(CH2SC6H4CH2OC5H2N(CH2OC5H2N(COOC2H5)2)2)2]Pd(η3-1,1-dimethylallyl)(CF3SO3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 12288-41-4
bis(μ-chloro)bis{(1,2,3-η)-3-methyl-2-butenyl}palladium

: 2923-28-6
silver trifluoromethanesulfonate

: 231955-83-2
C₆H₅CH₂OC₅H₂N(CH₂SC₆H₄CH₂OC₅H₂N(CH₂OC₅H₂N(COOC₂H₅)2)2)2

: 474976-24-4
[C6H5CH2OC5H2N(CH2SC6H4CH2OC5H2N(CH2OC5H2N(COOC2H5)2)2)2]Pd(η3-1,1-dimethylallyl)(CF3SO3)

Guidance literature:: With pyrographite; In dichloromethane; N2; addn. of silver salt to dichloromethane soln. of Pd complex, stirring in dark for 4 h, filtering, addn. of ligand, stirring for 30 min, treating with activated charcoal; filtering on Celite filter, pptn. by addn. of diethyl ether to a concd. soln. in ice bath; elem. anal.;
DOI:10.1021/om020391l