3-BUTOXY-4-METHOXYBENZALDEHYDE

Base Information

• Chemical Name: 3-BUTOXY-4-METHOXYBENZALDEHYDE
• CAS No.: 34127-96-3
• Molecular Formula: C12H16 O3
• Molecular Weight: 208.257
• Mol file: 34127-96-3.mol

Synonyms:3-Butoxy-4-methoxybenzaldehyde

Chemical Property of 3-BUTOXY-4-METHOXYBENZALDEHYDE

Chemical Property:

• Vapor Pressure: 0.00033mmHg at 25°C
• Boiling Point: 319.9°C at 760 mmHg
• Flash Point: 138.3°C
• PSA: 35.53000
• Density: 1.048g/cm³
• LogP: 2.68660

Purity/Quality:

98%Min ^*data from raw suppliers

3-butoxy-4-methoxybenzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-BUTOXY-4-METHOXYBENZALDEHYDE

There total 5 articles about 3-BUTOXY-4-METHOXYBENZALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

→ 3-butyloxy-4-methoxybenzaldehyde (34127-96-3)

Guidance literature:

Reference yield: 72.0%

isovanillin (621-59-0) + 1-bromo-butane (109-65-9) → 3-butyloxy-4-methoxybenzaldehyde (34127-96-3)

Guidance literature:

isovanillin; In N,N-dimethyl-formamide; for 0.166667h; Reflux; Alkaline conditions;

1-bromo-butane; In N,N-dimethyl-formamide; for 5h; Reflux;

DOI:10.1016/j.bioorg.2018.10.029

Reference yield:

isovanillin (621-59-0) + 1-iodo-butane (542-69-8) → 3-butyloxy-4-methoxybenzaldehyde (34127-96-3)

Guidance literature:

With potassium carbonate; In N-methyl-acetamide;

upstream raw materials:

isovanillin

1-bromo-butane

1-iodo-butane

2-methoxy-phenol

Downstream raw materials:

acide 3-n-butoxy-4-methoxybenzoique

isovanillin

C₁₂H₁₈O₃

5-(3-Butoxy-4-methoxy-phenyl)-thiazolidine-2,4-dione

Refernces

• 1、 Huang, Wei-Bin,Du, Cai-Yan,Jiang, Jian-An,Ji, Ya-Fei. "Concurrent synthesis of vanillin and isovanillin". . p. 2849 - 2856. Retrieved 2013/07/26.
• 2、 -. "PYRIMIDINE AND QUINAZOLINE DERIVATIVES". Page/Page column 78-79. . Retrieved 2008/06/13.