(1RS,2S,3S)-2,3-bis(tert-butyldiphenylsilyloxymethyl)cyclohex-5-en-1-ol

Base Information

Chemical Name:(1RS,2S,3S)-2,3-bis(tert-butyldiphenylsilyloxymethyl)cyclohex-5-en-1-ol
CAS No.:943003-63-2
Molecular Formula:C₄₀H₅₀O₃Si₂
Molecular Weight:635.006
Hs Code.:

Synonyms:(1RS,2S,3S)-2,3-bis(tert-butyldiphenylsilyloxymethyl)cyclohex-5-en-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1RS,2S,3S)-2,3-bis(tert-butyldiphenylsilyloxymethyl)cyclohex-5-en-1-ol

Chemical Property:

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Technology Process of (1RS,2S,3S)-2,3-bis(tert-butyldiphenylsilyloxymethyl)cyclohex-5-en-1-ol

There total 3 articles about (1RS,2S,3S)-2,3-bis(tert-butyldiphenylsilyloxymethyl)cyclohex-5-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 943003-61-0
C₄₀H₅₀O₂Si₂

: 943003-63-2
(1RS,2S,3S)-2,3-bis(tert-butyldiphenylsilyloxymethyl)cyclohex-5-en-1-ol

Guidance literature:: With selenium(IV) oxide; In 1,4-dioxane; water; at 90 ℃; for 36h;
DOI:10.1002/ejoc.200700068

Reference yield:

: C₂₈H₄₆O₄

: 943003-63-2
(1RS,2S,3S)-2,3-bis(tert-butyldiphenylsilyloxymethyl)cyclohex-5-en-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

2: 99 percent / imidazole / CH₂Cl₂ / 12 h / 0 - 20 °C

3: 54 percent / SeO₂ / dioxane; H₂O / 36 h / 90 °C

With 1H-imidazole; lithium aluminium tetrahydride; selenium(IV) oxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1002/ejoc.200700068

Reference yield:

: 15679-27-3
(4S,5S)-4,5-bis(hydroxymethyl)cyclohexene

: 943003-63-2
(1RS,2S,3S)-2,3-bis(tert-butyldiphenylsilyloxymethyl)cyclohex-5-en-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / imidazole / CH₂Cl₂ / 12 h / 0 - 20 °C

2: 54 percent / SeO₂ / dioxane; H₂O / 36 h / 90 °C

With 1H-imidazole; selenium(IV) oxide; In 1,4-dioxane; dichloromethane; water;
DOI:10.1002/ejoc.200700068