C₂₈H₂₂Cl₄N₈

Base Information

• Chemical Name: C₂₈H₂₂Cl₄N₈
• CAS No.: 1384471-14-0
• Molecular Formula: C₂₈H₂₂Cl₄N₈
• Molecular Weight: 612.348
• Mol file: 1384471-14-0.mol

Synonyms:C₂₈H₂₂Cl₄N₈

Chemical Property of C₂₈H₂₂Cl₄N₈

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₂₈H₂₂Cl₄N₈

There total 2 articles about C₂₈H₂₂Cl₄N₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

1,3,5-trichloro-2,4,6-triazine (108-77-0) + 3'-(3-aminophenyl)-5'-tert-butyl-[1,1'-biphenyl]-3-amine (1138835-40-1) → C28H22Cl4N8 (1384471-14-0)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 6h; Cooling with ice;

DOI:10.1016/j.tet.2012.04.108

Reference yield:

di-tert-butyl (5'-(tert-butyl)-[1,1':3',1''-terphenyl]-3,3''-diyl)dicarbamate (1384471-04-8) → C28H22Cl4N8 (1384471-14-0)

Guidance literature:

Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 24 h / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 6 h / 20 °C / Cooling with ice

With N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;

DOI:10.1016/j.tet.2012.04.108

upstream raw materials:

1,3,5-trichloro-2,4,6-triazine

3'-(3-aminophenyl)-5'-tert-butyl-[1,1'-biphenyl]-3-amine

di-tert-butyl (5'-(tert-butyl)-[1,1':3',1''-terphenyl]-3,3''-diyl)dicarbamate