C₅₃H₆₀O₇Si

Base Information

Chemical Name:C₅₃H₆₀O₇Si
CAS No.:1260148-67-1
Molecular Formula:C₅₃H₆₀O₇Si
Molecular Weight:837.141
Hs Code.:

C<sub>53</sub>H<sub>60</sub>O<sub>7</sub>Si

Synonyms:C₅₃H₆₀O₇Si

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Chemical Property of C₅₃H₆₀O₇Si

Chemical Property:

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Technology Process of C₅₃H₆₀O₇Si

There total 14 articles about C₅₃H₆₀O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 124-38-9,18923-20-1
carbon dioxide

: 1260148-55-7
C₄₅H₅₃IO₅Si

: 100-39-0
benzyl bromide

: 1260148-67-1
C₅₃H₆₀O₇Si

Guidance literature:: C₄₅H₅₃IO₅Si; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -110 ℃; for 0.0833333h; Inert atmosphere;

carbon dioxide; In tetrahydrofuran; pentane; at -110 - 0 ℃; for 1h; Inert atmosphere;

benzyl bromide; In acetonitrile; at 80 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ol102652t

Reference yield:

: 1141365-67-4
(3S,4S)-dihydro-4-[2-[(1,1-dimethylethyl)diphenylsilyloxy]ethyl]-3-methyl-2(3H)-furanone

: 1260148-67-1
C₅₃H₆₀O₇Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene / 24 h / 65 °C / Inert atmosphere

2.1: tert-butylmagnesium chloride / 3 h / -78 - 20 °C / Inert atmosphere

2.2: 20 °C

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / chloroform / 60 h / 60 °C / Inert atmosphere

4.1: CeCl₃*LiCl / tetrahydrofuran; diethyl ether / 0.75 h / 0 °C / Inert atmosphere

4.2: 0.75 h / -78 °C / Inert atmosphere

4.3: 0.25 h / -78 °C / Inert atmosphere

5.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.08 h / -110 °C / Inert atmosphere

5.2: 1 h / -110 - 0 °C / Inert atmosphere

5.3: 12 h / 80 °C / Inert atmosphere

With CeCl₃*LiCl; tert-butylmagnesium chloride; tert.-butyl lithium; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; chloroform; toluene; pentane;
DOI:10.1021/ol102652t

Reference yield:

: 1260148-61-5
methyl 2-(3,5-bis(benzyloxy)-2-formylphenyl)acetate

: 1260148-67-1
C₅₃H₆₀O₇Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere

1.2: 0 °C

2.1: Me₄N(ICl₂); sodium hydrogencarbonate / dichloromethane / 16 h / 0 °C / Inert atmosphere

3.1: sodium tetrahydroborate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3.2: 0 °C

4.1: tert-butylmagnesium chloride / 3 h / -78 - 20 °C / Inert atmosphere

4.2: 20 °C

5.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / chloroform / 60 h / 60 °C / Inert atmosphere

6.1: CeCl₃*LiCl / tetrahydrofuran; diethyl ether / 0.75 h / 0 °C / Inert atmosphere

6.2: 0.75 h / -78 °C / Inert atmosphere

6.3: 0.25 h / -78 °C / Inert atmosphere

7.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.08 h / -110 °C / Inert atmosphere

7.2: 1 h / -110 - 0 °C / Inert atmosphere

7.3: 12 h / 80 °C / Inert atmosphere

With sodium tetrahydroborate; Me₄N(ICl₂); CeCl₃*LiCl; tert-butylmagnesium chloride; tert.-butyl lithium; boron tribromide; sodium hydrogencarbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; dichloromethane; chloroform; pentane;
DOI:10.1021/ol102652t