bis(11-(N-tert butyl-α-(4-benzoyloxy-phenyl))undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate

Base Information

Chemical Name:bis(11-(N-tert butyl-α-(4-benzoyloxy-phenyl))undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate
CAS No.:1303962-76-6
Molecular Formula:C₅₇H₇₈N₂O₁₁
Molecular Weight:967.253
Hs Code.:

Synonyms:bis(11-(N-tert butyl-α-(4-benzoyloxy-phenyl))undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate

Suppliers and Price of bis(11-(N-tert butyl-α-(4-benzoyloxy-phenyl))undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of bis(11-(N-tert butyl-α-(4-benzoyloxy-phenyl))undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of bis(11-(N-tert butyl-α-(4-benzoyloxy-phenyl))undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate

There total 4 articles about bis(11-(N-tert butyl-α-(4-benzoyloxy-phenyl))undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1303962-75-5
bis(11-(4-formylbenzoyloxy)undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate

: 253605-31-1
N-tertiary butyl hydroxyl amine acetate

: 1303962-76-6
bis(11-(N-tert butyl-α-(4-benzoyloxy-phenyl))undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate

Guidance literature:: With sodium sulfate; N-ethyl-N,N-diisopropylamine; In chloroform; at 20 ℃; for 48h; Darkness;
DOI:10.1039/c1cc10322a

Reference yield:

: 1611-56-9
1-Bromo-11-hydroxyundecane

: 1303962-76-6
bis(11-(N-tert butyl-α-(4-benzoyloxy-phenyl))undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 16 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 24 h / Reflux

3: sodium sulfate; N-ethyl-N,N-diisopropylamine / chloroform / 48 h / 20 °C / Darkness

With potassium carbonate; sodium sulfate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1039/c1cc10322a

Reference yield:

: 1114540-72-5
5-(prop-2-ynyloxy)isophthaloyl dichloride

: 1303962-76-6
bis(11-(N-tert butyl-α-(4-benzoyloxy-phenyl))undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 16 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 24 h / Reflux

3: sodium sulfate; N-ethyl-N,N-diisopropylamine / chloroform / 48 h / 20 °C / Darkness

With potassium carbonate; sodium sulfate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1039/c1cc10322a