bis(11-(4-formylbenzoyloxy)undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate

Base Information

Chemical Name:bis(11-(4-formylbenzoyloxy)undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate
CAS No.:1303962-75-5
Molecular Formula:C₄₉H₆₀O₁₁
Molecular Weight:825.009
Hs Code.:

Synonyms:bis(11-(4-formylbenzoyloxy)undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(11-(4-formylbenzoyloxy)undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate

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Technology Process of bis(11-(4-formylbenzoyloxy)undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate

There total 3 articles about bis(11-(4-formylbenzoyloxy)undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1303962-74-4
bis(11-bromoundecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate

: 619-66-9
4-Carboxybenzaldehyde

: 1303962-75-5
bis(11-(4-formylbenzoyloxy)undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 24h; Reflux;
DOI:10.1039/c1cc10322a

Reference yield:

: 1611-56-9
1-Bromo-11-hydroxyundecane

: 1303962-75-5
bis(11-(4-formylbenzoyloxy)undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 16 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 24 h / Reflux

With potassium carbonate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c1cc10322a

Reference yield:

: 1114540-72-5
5-(prop-2-ynyloxy)isophthaloyl dichloride

: 1303962-75-5
bis(11-(4-formylbenzoyloxy)undecyl) 5-(prop-2-ynyloxy)benzene-1,3-dioate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 16 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 24 h / Reflux

With potassium carbonate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c1cc10322a