1-[2-(3-carbonylphenoxy)-5-methoxyphenyl]-2-{4-methoxy-3-[2-methoxy-5-(hydroxymethyl)phenyl]phenyl}ethane

Base Information

Chemical Name:1-[2-(3-carbonylphenoxy)-5-methoxyphenyl]-2-{4-methoxy-3-[2-methoxy-5-(hydroxymethyl)phenyl]phenyl}ethane
CAS No.:189289-15-4
Molecular Formula:C₃₁H₃₀O₆
Molecular Weight:498.576
Hs Code.:

Synonyms:1-[2-(3-carbonylphenoxy)-5-methoxyphenyl]-2-{4-methoxy-3-[2-methoxy-5-(hydroxymethyl)phenyl]phenyl}ethane

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Chemical Property of 1-[2-(3-carbonylphenoxy)-5-methoxyphenyl]-2-{4-methoxy-3-[2-methoxy-5-(hydroxymethyl)phenyl]phenyl}ethane

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Technology Process of 1-[2-(3-carbonylphenoxy)-5-methoxyphenyl]-2-{4-methoxy-3-[2-methoxy-5-(hydroxymethyl)phenyl]phenyl}ethane

There total 4 articles about 1-[2-(3-carbonylphenoxy)-5-methoxyphenyl]-2-{4-methoxy-3-[2-methoxy-5-(hydroxymethyl)phenyl]phenyl}ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 189289-14-3
1-[2-(3-carbonylphenoxy)-5-methoxyphenyl]-2-[4-methoxy-3-(2-methoxy-5-{[(tetrahydropyran-2-yl)oxy]methyl}phenyl)phenyl]ethane

: 189289-15-4
1-[2-(3-carbonylphenoxy)-5-methoxyphenyl]-2-{4-methoxy-3-[2-methoxy-5-(hydroxymethyl)phenyl]phenyl}ethane

Guidance literature:: With Amberlite IR 120; In ethanol; for 1h; Heating;
DOI:10.1021/jo9620829

Reference yield:

: 1-{5-methoxy-2-[3-(methoxycarbonyl)phenoxy]phenyl}-2-[4-methoxy-3-(2-methoxy-5-{[(tetrahydropyran-2-yl)oxy]methyl}phenyl)phenyl]ethene

: 189289-15-4
1-[2-(3-carbonylphenoxy)-5-methoxyphenyl]-2-{4-methoxy-3-[2-methoxy-5-(hydroxymethyl)phenyl]phenyl}ethane

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / H₂ / Pd/C / ethanol

2: 92 percent / LiAlH₄ / diethyl ether

3: 51 percent / PCC, NaOAc / CH₂Cl₂ / 1 h

4: 36 percent / Amberlite IR 120 / ethanol / 1 h / Heating

With lithium aluminium tetrahydride; Amberlite IR 120; hydrogen; sodium acetate; pyridinium chlorochromate; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jo9620829

Reference yield:

: 189289-12-1
1-{5-methoxy-2-[3-(methoxycarbonyl)phenoxy]phenyl}-2-[4-methoxy-3-(2-methoxy-5-{[(tetrahydropyran-2-yl)oxy]methyl}phenyl)phenyl]ethane

: 189289-15-4
1-[2-(3-carbonylphenoxy)-5-methoxyphenyl]-2-{4-methoxy-3-[2-methoxy-5-(hydroxymethyl)phenyl]phenyl}ethane

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / LiAlH₄ / diethyl ether

2: 51 percent / PCC, NaOAc / CH₂Cl₂ / 1 h

3: 36 percent / Amberlite IR 120 / ethanol / 1 h / Heating

With lithium aluminium tetrahydride; Amberlite IR 120; sodium acetate; pyridinium chlorochromate; In diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jo9620829