1-{5-methoxy-2-[3-(methoxycarbonyl)phenoxy]phenyl}-2-[4-methoxy-3-(2-methoxy-5-{[(tetrahydropyran-2-yl)oxy]methyl}phenyl)phenyl]ethane

Base Information

Chemical Name:1-{5-methoxy-2-[3-(methoxycarbonyl)phenoxy]phenyl}-2-[4-methoxy-3-(2-methoxy-5-{[(tetrahydropyran-2-yl)oxy]methyl}phenyl)phenyl]ethane
CAS No.:189289-12-1
Molecular Formula:C₃₇H₄₀O₈
Molecular Weight:612.72
Hs Code.:

Synonyms:1-{5-methoxy-2-[3-(methoxycarbonyl)phenoxy]phenyl}-2-[4-methoxy-3-(2-methoxy-5-{[(tetrahydropyran-2-yl)oxy]methyl}phenyl)phenyl]ethane

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Chemical Property of 1-{5-methoxy-2-[3-(methoxycarbonyl)phenoxy]phenyl}-2-[4-methoxy-3-(2-methoxy-5-{[(tetrahydropyran-2-yl)oxy]methyl}phenyl)phenyl]ethane

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Technology Process of 1-{5-methoxy-2-[3-(methoxycarbonyl)phenoxy]phenyl}-2-[4-methoxy-3-(2-methoxy-5-{[(tetrahydropyran-2-yl)oxy]methyl}phenyl)phenyl]ethane

There total 1 articles about 1-{5-methoxy-2-[3-(methoxycarbonyl)phenoxy]phenyl}-2-[4-methoxy-3-(2-methoxy-5-{[(tetrahydropyran-2-yl)oxy]methyl}phenyl)phenyl]ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1-{5-methoxy-2-[3-(methoxycarbonyl)phenoxy]phenyl}-2-[4-methoxy-3-(2-methoxy-5-{[(tetrahydropyran-2-yl)oxy]methyl}phenyl)phenyl]ethene

: 189289-12-1
1-{5-methoxy-2-[3-(methoxycarbonyl)phenoxy]phenyl}-2-[4-methoxy-3-(2-methoxy-5-{[(tetrahydropyran-2-yl)oxy]methyl}phenyl)phenyl]ethane

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1021/jo9620829

Reference yield: 92.0%

: 189289-12-1
1-{5-methoxy-2-[3-(methoxycarbonyl)phenoxy]phenyl}-2-[4-methoxy-3-(2-methoxy-5-{[(tetrahydropyran-2-yl)oxy]methyl}phenyl)phenyl]ethane

: 189289-13-2
1-{5-methoxy-2-[3-(hydroxymethyl)phenoxy]phenyl}-2-[4-methoxy-3-(2-methoxy-5-{[(tetrahydropyran-2-yl)oxy]methyl}phenyl)phenyl]ethane

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1021/jo9620829

Reference yield:

: 189289-12-1
1-{5-methoxy-2-[3-(methoxycarbonyl)phenoxy]phenyl}-2-[4-methoxy-3-(2-methoxy-5-{[(tetrahydropyran-2-yl)oxy]methyl}phenyl)phenyl]ethane

: 189289-15-4
1-[2-(3-carbonylphenoxy)-5-methoxyphenyl]-2-{4-methoxy-3-[2-methoxy-5-(hydroxymethyl)phenyl]phenyl}ethane

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / LiAlH₄ / diethyl ether

2: 51 percent / PCC, NaOAc / CH₂Cl₂ / 1 h

3: 36 percent / Amberlite IR 120 / ethanol / 1 h / Heating

With lithium aluminium tetrahydride; Amberlite IR 120; sodium acetate; pyridinium chlorochromate; In diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jo9620829