(14R,18R)-14-(benzyloxycarbonylamino)-18-(octylcarbamoyloxy )-13,21-dioxo-3,6,9,20-tetraoxa-16-thia-12,22-diazatriacontylphosphonic acid diethyl ester

Base Information

Chemical Name:(14R,18R)-14-(benzyloxycarbonylamino)-18-(octylcarbamoyloxy )-13,21-dioxo-3,6,9,20-tetraoxa-16-thia-12,22-diazatriacontylphosphonic acid diethyl ester
CAS No.:1337527-69-1
Molecular Formula:C₄₄H₇₉N₄O₁₃PS
Molecular Weight:935.17
Hs Code.:

(14R,18R)-14-(benzyloxycarbonylamino)-18-(octylcarbamoyloxy )-13,21-dioxo-3,6,9,20-tetraoxa-16-thia-12,22-diazatriacontylphosphonic acid diethyl ester

Synonyms:(14R,18R)-14-(benzyloxycarbonylamino)-18-(octylcarbamoyloxy )-13,21-dioxo-3,6,9,20-tetraoxa-16-thia-12,22-diazatriacontylphosphonic acid diethyl ester

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Chemical Property of (14R,18R)-14-(benzyloxycarbonylamino)-18-(octylcarbamoyloxy )-13,21-dioxo-3,6,9,20-tetraoxa-16-thia-12,22-diazatriacontylphosphonic acid diethyl ester

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Technology Process of (14R,18R)-14-(benzyloxycarbonylamino)-18-(octylcarbamoyloxy )-13,21-dioxo-3,6,9,20-tetraoxa-16-thia-12,22-diazatriacontylphosphonic acid diethyl ester

There total 10 articles about (14R,18R)-14-(benzyloxycarbonylamino)-18-(octylcarbamoyloxy )-13,21-dioxo-3,6,9,20-tetraoxa-16-thia-12,22-diazatriacontylphosphonic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1337527-25-9
diethyl (2-(2-(2-(2-aminoethoxy)ethoxy)ethoxy)ethyl)phosphonate

: 1337527-63-5
(R)-2-(benzyloxycarbonylamino )-3-((R)-2,3-bis(octylcarbamoyloxy)propylthio)propanoic acid

: 1337527-69-1
(14R,18R)-14-(benzyloxycarbonylamino)-18-(octylcarbamoyloxy )-13,21-dioxo-3,6,9,20-tetraoxa-16-thia-12,22-diazatriacontylphosphonic acid diethyl ester

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 4h;

Reference yield:

: 638-56-2,27252-69-3
1,11-dichloro-3,6,9-trioxaundecane

: 1337527-69-1
(14R,18R)-14-(benzyloxycarbonylamino)-18-(octylcarbamoyloxy )-13,21-dioxo-3,6,9,20-tetraoxa-16-thia-12,22-diazatriacontylphosphonic acid diethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: sodium iodide / acetone / 80 °C / Sealed vial

2: 0.33 h / 160 °C / Microwave

3: sodium azide / N,N-dimethyl-formamide / 50 °C

4: hydrogen / palladium(II) hydroxide / ethanol / 4 h / 760.05 Torr

5: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 4 h / 20 °C

With sodium azide; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; sodium iodide; palladium(II) hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide; acetone;

Reference yield:

: 36839-56-2
1,11-diiodo-3,6-9-trioxaundecane

: 1337527-69-1
(14R,18R)-14-(benzyloxycarbonylamino)-18-(octylcarbamoyloxy )-13,21-dioxo-3,6,9,20-tetraoxa-16-thia-12,22-diazatriacontylphosphonic acid diethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 0.33 h / 160 °C / Microwave

2: sodium azide / N,N-dimethyl-formamide / 50 °C

3: hydrogen / palladium(II) hydroxide / ethanol / 4 h / 760.05 Torr

4: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 4 h / 20 °C

With sodium azide; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; palladium(II) hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;