2-methoxy-4-(3-methyl-5-oxo-1-phenyl-4-pyrazolylidenemethyl)phenoxyacetic acid

Base Information

Chemical Name:2-methoxy-4-(3-methyl-5-oxo-1-phenyl-4-pyrazolylidenemethyl)phenoxyacetic acid
CAS No.:81836-88-6
Molecular Formula:C₂₀H₁₈N₂O₅
Molecular Weight:366.373
Hs Code.:

Synonyms:2-methoxy-4-(3-methyl-5-oxo-1-phenyl-4-pyrazolylidenemethyl)phenoxyacetic acid

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Chemical Property of 2-methoxy-4-(3-methyl-5-oxo-1-phenyl-4-pyrazolylidenemethyl)phenoxyacetic acid

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Technology Process of 2-methoxy-4-(3-methyl-5-oxo-1-phenyl-4-pyrazolylidenemethyl)phenoxyacetic acid

There total 3 articles about 2-methoxy-4-(3-methyl-5-oxo-1-phenyl-4-pyrazolylidenemethyl)phenoxyacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1660-19-1
(4-formyl-2-methoxyphenoxy)acetic acid

: 89-25-8
edaravone

: 81836-88-6
2-methoxy-4-(3-methyl-5-oxo-1-phenyl-4-pyrazolylidenemethyl)phenoxyacetic acid

Guidance literature:: With sodium acetate; acetic anhydride; In acetic acid; for 0.75h; Heating;

Reference yield: 70.0%

: 81836-90-0
5-methyl-2-phenyl-4-vanillylidene-2,4-dihydro-pyrazol-3-one

: 79-11-8
chloroacetic acid

: 81836-88-6
2-methoxy-4-(3-methyl-5-oxo-1-phenyl-4-pyrazolylidenemethyl)phenoxyacetic acid

Guidance literature:: In potassium hydroxide; for 4h; Heating;

Reference yield:

: 89-25-8
edaravone

: 81836-88-6
2-methoxy-4-(3-methyl-5-oxo-1-phenyl-4-pyrazolylidenemethyl)phenoxyacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / CH₃COONa, Ac₂O / acetic acid / 0.75 h / Heating

2: 70 percent / aq. KOH / 4 h / Heating

With sodium acetate; acetic anhydride; In potassium hydroxide; acetic acid;