N-(tert-butyloxycarbonyl)-3-(3-formyl-4-methoxy-5-methylphenyl)-L-alanine ethyl ester

Base Information

Chemical Name:N-(tert-butyloxycarbonyl)-3-(3-formyl-4-methoxy-5-methylphenyl)-L-alanine ethyl ester
CAS No.:699536-25-9
Molecular Formula:C₁₉H₂₇NO₆
Molecular Weight:365.426
Hs Code.:

Synonyms:N-(tert-butyloxycarbonyl)-3-(3-formyl-4-methoxy-5-methylphenyl)-L-alanine ethyl ester

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Chemical Property of N-(tert-butyloxycarbonyl)-3-(3-formyl-4-methoxy-5-methylphenyl)-L-alanine ethyl ester

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Technology Process of N-(tert-butyloxycarbonyl)-3-(3-formyl-4-methoxy-5-methylphenyl)-L-alanine ethyl ester

There total 2 articles about N-(tert-butyloxycarbonyl)-3-(3-formyl-4-methoxy-5-methylphenyl)-L-alanine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 74-88-4
methyl iodide

: 699536-24-8
N-(tert-butyloxycarbonyl)-3-(3-formyl-4-hydroxy-5-methylphenyl)-L-alanine ethyl ester

: 699536-25-9
N-(tert-butyloxycarbonyl)-3-(3-formyl-4-methoxy-5-methylphenyl)-L-alanine ethyl ester

Guidance literature:: With potassium carbonate; In acetone; at 50 ℃;
DOI:10.1016/j.tetlet.2004.03.112

Reference yield: 82.0%

: 1361398-95-9
C₁₈H₂₄INO₆

: 594-27-4
tetramethylstannane

: 699536-25-9
N-(tert-butyloxycarbonyl)-3-(3-formyl-4-methoxy-5-methylphenyl)-L-alanine ethyl ester

Guidance literature:: With 1-methyl-pyrrolidin-2-one; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; at 70 ℃; for 71h;
DOI:10.2174/157017811799304160

Reference yield:

: 699536-25-9
N-(tert-butyloxycarbonyl)-3-(3-formyl-4-methoxy-5-methylphenyl)-L-alanine ethyl ester

: 2-tert-butoxycarbonylamino-3-(3-hydroxy-4-methoxy-5-methyl-phenyl)-propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide; water / dimethylformamide / 20 °C

2: diphenyldiselenide; hydrogen peroxide; 18-crown-6 / K₂HPO₄ / CH₂Cl₂; H₂O / 20 °C

With lithium hydroxide; 18-crown-6 ether; diphenyl diselenide; water; dihydrogen peroxide; dipotassium hydrogenphosphate; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2004.03.112