4,4'-diacryloylphenyl ether

Base Information

• Chemical Name: 4,4'-diacryloylphenyl ether
• CAS No.: 17662-13-4
• Molecular Formula: C₁₈H₁₄O₃
• Molecular Weight: 278.307
• Mol file: 17662-13-4.mol

Synonyms:4,4'-diacryloylphenyl ether

Chemical Property of 4,4'-diacryloylphenyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,4'-diacryloylphenyl ether

There total 3 articles about 4,4'-diacryloylphenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

diphenylether (101-84-8) + acryloyl chloride (814-68-6,25189-84-8) → 4,4'-diacryloylphenyl ether (17662-13-4)

Guidance literature:

With aluminum (III) chloride; In dichloromethane; at 0 ℃; for 4h; Inert atmosphere;

DOI:10.1002/bkcs.10586

Reference yield:

diphenylether (101-84-8) → 4,4'-diacryloylphenyl ether (17662-13-4)

Guidance literature:

Multi-step reaction with 2 steps

1: AlCl₃ / CH₂Cl₂ / Heating

2: H₂SO₄

With aluminium trichloride; sulfuric acid; In dichloromethane;

Reference yield:

Bis-p-(ω-hydroxypropanoyl)-phenyloxid (31825-79-3) → 4,4'-diacryloylphenyl ether (17662-13-4)

Guidance literature:

With sulfuric acid;

upstream raw materials:

Bis-p-(ω-hydroxypropanoyl)-phenyloxid

diphenylether

acryloyl chloride