6-chloro-2-methoxy-9-(2-amino-4,5-dimethylanilino)acridine hydrochloride

Base Information

Chemical Name:6-chloro-2-methoxy-9-(2-amino-4,5-dimethylanilino)acridine hydrochloride
CAS No.:1610849-75-6
Molecular Formula:C₂₂H₂₀ClN₃O*ClH
Molecular Weight:414.334
Hs Code.:

Synonyms:6-chloro-2-methoxy-9-(2-amino-4,5-dimethylanilino)acridine hydrochloride

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Chemical Property of 6-chloro-2-methoxy-9-(2-amino-4,5-dimethylanilino)acridine hydrochloride

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Technology Process of 6-chloro-2-methoxy-9-(2-amino-4,5-dimethylanilino)acridine hydrochloride

There total 4 articles about 6-chloro-2-methoxy-9-(2-amino-4,5-dimethylanilino)acridine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 86-38-4
6,9-dichloro-2-methoxyacridine

: 3171-45-7
4,5-dimethyl-1,2-phenylenediamine

: 1610849-75-6
6-chloro-2-methoxy-9-(2-amino-4,5-dimethylanilino)acridine hydrochloride

Guidance literature:: In methanol; at 110 ℃; for 0.166667h; Microwave irradiation;
DOI:10.1016/j.tetlet.2014.04.035

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1610849-75-6
6-chloro-2-methoxy-9-(2-amino-4,5-dimethylanilino)acridine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: copper; potassium carbonate / N,N-dimethyl-formamide / Heating

2: trichlorophosphate / 0.25 h / 140 °C / Microwave irradiation

3: methanol / 0.17 h / 110 °C / Microwave irradiation

With copper; potassium carbonate; trichlorophosphate; In methanol; N,N-dimethyl-formamide; 1: |Goldberg Reaction;
DOI:10.1016/j.tetlet.2014.04.035

Reference yield:

: 50-84-0
2,4 dichlorobenzoic acid

: 1610849-75-6
6-chloro-2-methoxy-9-(2-amino-4,5-dimethylanilino)acridine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: copper; potassium carbonate / N,N-dimethyl-formamide / Heating

2: trichlorophosphate / 0.25 h / 140 °C / Microwave irradiation

3: methanol / 0.17 h / 110 °C / Microwave irradiation

With copper; potassium carbonate; trichlorophosphate; In methanol; N,N-dimethyl-formamide; 1: |Goldberg Reaction;
DOI:10.1016/j.tetlet.2014.04.035