N-[2-amino-6-(benzyloxy)-5-nitrosopyrimidin-4-yl]-3-(phthalimido)propanamide

Base Information

Chemical Name:N-[2-amino-6-(benzyloxy)-5-nitrosopyrimidin-4-yl]-3-(phthalimido)propanamide
CAS No.:1182207-19-7
Molecular Formula:C₂₂H₁₈N₆O₅
Molecular Weight:446.422
Hs Code.:

Synonyms:N-[2-amino-6-(benzyloxy)-5-nitrosopyrimidin-4-yl]-3-(phthalimido)propanamide

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Chemical Property of N-[2-amino-6-(benzyloxy)-5-nitrosopyrimidin-4-yl]-3-(phthalimido)propanamide

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Technology Process of N-[2-amino-6-(benzyloxy)-5-nitrosopyrimidin-4-yl]-3-(phthalimido)propanamide

There total 1 articles about N-[2-amino-6-(benzyloxy)-5-nitrosopyrimidin-4-yl]-3-(phthalimido)propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 17137-11-0
3-phthalimidopropionyl chloride

: 101724-61-2
2,4-diamino-6-(benzyloxy)-5-nitrosopyrimidine

: 1182207-19-7
N-[2-amino-6-(benzyloxy)-5-nitrosopyrimidin-4-yl]-3-(phthalimido)propanamide

Guidance literature:: In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/hlca.200900047

Reference yield: 51.0%

: 107-59-5
tert-Butyl chloroacetate

: 1182207-19-7
N-[2-amino-6-(benzyloxy)-5-nitrosopyrimidin-4-yl]-3-(phthalimido)propanamide

: 1182207-21-1
tert-butyl 6-O-benzyl-8-(2-phthalimidoethyl)guanine-9-acetate

: 1182207-22-2
tert-butyl 6-O-benzyl-8-(2-phthalimidoethyl)guanine-7-acetate

Guidance literature:: N-[2-amino-6-(benzyloxy)-5-nitrosopyrimidin-4-yl]-3-(phthalimido)propanamide; With trimethylphosphane; In tetrahydrofuran; toluene; at 60 ℃; for 4h; Sonication; Inert atmosphere;

tert-Butyl chloroacetate; With potassium carbonate; caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1002/hlca.200900047

Reference yield:

: 1182207-19-7
N-[2-amino-6-(benzyloxy)-5-nitrosopyrimidin-4-yl]-3-(phthalimido)propanamide

: 1182207-20-0
C₂₂H₁₈N₆O₃

Guidance literature:: With trimethylphosphane; In tetrahydrofuran; toluene; at 60 ℃; for 4h; Sonication; Inert atmosphere;
DOI:10.1002/hlca.200900047