4⁽⁵⁾-diphenylhydroxymethylimidazole hydrochloride

Base Information

Chemical Name:4⁽⁵⁾-diphenylhydroxymethylimidazole hydrochloride
CAS No.:131977-00-9
Molecular Formula:C₁₆H₁₄N₂O*ClH
Molecular Weight:286.761
Hs Code.:

4<sup>(5)</sup>-diphenylhydroxymethylimidazole hydrochloride

Synonyms:4⁽⁵⁾-diphenylhydroxymethylimidazole hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4⁽⁵⁾-diphenylhydroxymethylimidazole hydrochloride

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Technology Process of 4⁽⁵⁾-diphenylhydroxymethylimidazole hydrochloride

There total 3 articles about 4⁽⁵⁾-diphenylhydroxymethylimidazole hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.8%

: 132287-57-1
4-diphenylhydroxymethyl-1-methoxymethyl-imidazole

: 131977-00-9
4⁽⁵⁾-diphenylhydroxymethylimidazole hydrochloride

Guidance literature:: With hydrogenchloride; for 20h; Heating;
DOI:10.1016/0223-5234(90)90180-B

Reference yield:

: 119-61-9
benzophenone

: 131977-00-9
4⁽⁵⁾-diphenylhydroxymethylimidazole hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA / 1.) THF, -65 deg C, 30 min, 2.) from -65 deg C to 20 deg C

2: 61.5 percent / aluminium amalgam / aq. ethanol / 42 h

3: 44.8 percent / 5 N HCl / 20 h / Heating

With hydrogenchloride; aluminium amalgam; lithium diisopropyl amide; In ethanol;
DOI:10.1016/0223-5234(90)90180-B

Reference yield:

: 132287-56-0
4-diphenylhydroxymethyl-1-methoxymethyl-2-phenylthioimidazole

: 131977-00-9
4⁽⁵⁾-diphenylhydroxymethylimidazole hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 61.5 percent / aluminium amalgam / aq. ethanol / 42 h

2: 44.8 percent / 5 N HCl / 20 h / Heating

With hydrogenchloride; aluminium amalgam; In ethanol;
DOI:10.1016/0223-5234(90)90180-B