[4-(Benzhydrylidene-amino)-phenyl]-[4-({4-[(4-bromo-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-tert-butoxycarbonyl-amino)-phenyl]-carbamic acid tert-butyl ester

Base Information

Chemical Name:[4-(Benzhydrylidene-amino)-phenyl]-[4-({4-[(4-bromo-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-tert-butoxycarbonyl-amino)-phenyl]-carbamic acid tert-butyl ester
CAS No.:206656-47-5
Molecular Formula:C₅₂H₅₃BrN₄O₆
Molecular Weight:909.92
Hs Code.:

[4-(Benzhydrylidene-amino)-phenyl]-[4-({4-[(4-bromo-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-tert-butoxycarbonyl-amino)-phenyl]-carbamic acid tert-butyl ester

Synonyms:[4-(Benzhydrylidene-amino)-phenyl]-[4-({4-[(4-bromo-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-tert-butoxycarbonyl-amino)-phenyl]-carbamic acid tert-butyl ester

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Chemical Property of [4-(Benzhydrylidene-amino)-phenyl]-[4-({4-[(4-bromo-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-tert-butoxycarbonyl-amino)-phenyl]-carbamic acid tert-butyl ester

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Technology Process of [4-(Benzhydrylidene-amino)-phenyl]-[4-({4-[(4-bromo-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-tert-butoxycarbonyl-amino)-phenyl]-carbamic acid tert-butyl ester

There total 1 articles about [4-(Benzhydrylidene-amino)-phenyl]-[4-({4-[(4-bromo-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-tert-butoxycarbonyl-amino)-phenyl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 200395-40-0
(4-{[4-(Benzhydrylidene-amino)-phenyl]-tert-butoxycarbonyl-amino}-phenyl)-{4-[tert-butoxycarbonyl-(4-trimethylsilanyl-phenyl)-amino]-phenyl}-carbamic acid tert-butyl ester

: 206656-47-5
[4-(Benzhydrylidene-amino)-phenyl]-[4-({4-[(4-bromo-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-tert-butoxycarbonyl-amino)-phenyl]-carbamic acid tert-butyl ester

Guidance literature:: With bromine; sodium acetate; In tetrahydrofuran; at 0 ℃; for 0.333333h;
DOI:10.1021/ja980052c

Reference yield: 85.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 206656-47-5
[4-(Benzhydrylidene-amino)-phenyl]-[4-({4-[(4-bromo-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-tert-butoxycarbonyl-amino)-phenyl]-carbamic acid tert-butyl ester

: {4-[(4-amino-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-[4-(tert-butoxycarbonyl-{4-[tert-butoxycarbonyl-(4-trimethylsilanyl-phenyl)-amino]-phenyl}-amino)-phenyl]-carbamic acid tert-butyl ester

: C₁₁₀H₁₂₇N₉O₁₆Si

Guidance literature:: [4-(Benzhydrylidene-amino)-phenyl]-[4-({4-[(4-bromo-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-tert-butoxycarbonyl-amino)-phenyl]-carbamic acid tert-butyl ester; {4-[(4-amino-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-[4-(tert-butoxycarbonyl-{4-[tert-butoxycarbonyl-(4-trimethylsilanyl-phenyl)-amino]-phenyl}-amino)-phenyl]-carbamic acid tert-butyl ester; With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; johnphos; sodium t-butanolate; In toluene; at 60 ℃; for 8h;

di-tert-butyl dicarbonate; With dmap; In tetrahydrofuran; at 60 ℃; Further stages.;
DOI:10.1021/jo991699y

Reference yield:

: 206656-46-4
{4-[(4-Amino-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-{4-[tert-butoxycarbonyl-(4-trimethylsilanyl-phenyl)-amino]-phenyl}-carbamic acid tert-butyl ester

: 206656-47-5
[4-(Benzhydrylidene-amino)-phenyl]-[4-({4-[(4-bromo-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-tert-butoxycarbonyl-amino)-phenyl]-carbamic acid tert-butyl ester

: C₉₄H₁₀₆N₈O₁₂Si

Guidance literature:: With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; (S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine); sodium t-butanolate; In toluene; at 65 ℃; for 17h;
DOI:10.1021/ja980052c