1D-2,6-O-bis(methoxymethylene)-myo-inositol 3,4,5-tris(dibenzyl phosphate)

Base Information

Chemical Name:1D-2,6-O-bis(methoxymethylene)-myo-inositol 3,4,5-tris(dibenzyl phosphate)
CAS No.:496808-75-4
Molecular Formula:C₅₂H₅₉O₁₇P₃
Molecular Weight:1048.95
Hs Code.:

Synonyms:1D-2,6-O-bis(methoxymethylene)-myo-inositol 3,4,5-tris(dibenzyl phosphate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1D-2,6-O-bis(methoxymethylene)-myo-inositol 3,4,5-tris(dibenzyl phosphate)

Chemical Property:

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Technology Process of 1D-2,6-O-bis(methoxymethylene)-myo-inositol 3,4,5-tris(dibenzyl phosphate)

There total 8 articles about 1D-2,6-O-bis(methoxymethylene)-myo-inositol 3,4,5-tris(dibenzyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 496808-74-3
1D-1-O-(tert-butyldiphenylsilyl)-2,6-O-bis(methoxymethylene)-myo-inositol 3,4,5-tris(dibenzyl phosphate)

: 496808-75-4
1D-2,6-O-bis(methoxymethylene)-myo-inositol 3,4,5-tris(dibenzyl phosphate)

Guidance literature:: With tetrabutyl ammonium fluoride; In N,N-dimethyl-formamide; for 1h;
DOI:10.1021/jo0206418

Reference yield:

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: 496808-75-4
1D-2,6-O-bis(methoxymethylene)-myo-inositol 3,4,5-tris(dibenzyl phosphate)

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrazole / acetonitrile / 6 h

1.2: 84 percent / 3-chloroperoxybenzoic acid / acetonitrile; CHCl₃ / -20 °C

2.1: 95 percent / tetra-n-butylammonium fluoride / dimethylformamide / 1 h

With 1H-tetrazole; tetrabutyl ammonium fluoride; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo0206418

Reference yield:

: 331679-26-6
2,3-O-(D-1,7,7-trimethylbicyclo[2.2.1]hept-6-ylidene)-D-myo-inositol

: 496808-75-4
1D-2,6-O-bis(methoxymethylene)-myo-inositol 3,4,5-tris(dibenzyl phosphate)

Guidance literature:: Multi-step reaction with 7 steps

1.1: 88 percent / imidazole

2.1: 90 percent / HSCH₂CH₂OH; BF₃*Et₂O

3.1: 92 percent / pyridine / -40 °C

4.1: 75 percent / diisopropylethylamine / dimethylformamide

5.1: 96 percent / methylamine / CHCl₃; ethanol / 48 h / 50 °C

6.1: tetrazole / acetonitrile / 6 h

6.2: 84 percent / 3-chloroperoxybenzoic acid / acetonitrile; CHCl₃ / -20 °C

7.1: 95 percent / tetra-n-butylammonium fluoride / dimethylformamide / 1 h

With pyridine; 1H-imidazole; 1H-tetrazole; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; methylamine; 2-hydroxyethanethiol; In ethanol; chloroform; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo0206418