toluene-4-sulfonic acid 3-{4-[2-(4-(dimethylamino)phenyl)vinyl]phenoxy}-2-hydroxymethylpropyl ester

Base Information

Chemical Name:toluene-4-sulfonic acid 3-{4-[2-(4-(dimethylamino)phenyl)vinyl]phenoxy}-2-hydroxymethylpropyl ester
CAS No.:902143-06-0
Molecular Formula:C₂₇H₃₁NO₅S
Molecular Weight:481.613
Hs Code.:

Synonyms:toluene-4-sulfonic acid 3-{4-[2-(4-(dimethylamino)phenyl)vinyl]phenoxy}-2-hydroxymethylpropyl ester

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Chemical Property of toluene-4-sulfonic acid 3-{4-[2-(4-(dimethylamino)phenyl)vinyl]phenoxy}-2-hydroxymethylpropyl ester

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Technology Process of toluene-4-sulfonic acid 3-{4-[2-(4-(dimethylamino)phenyl)vinyl]phenoxy}-2-hydroxymethylpropyl ester

There total 2 articles about toluene-4-sulfonic acid 3-{4-[2-(4-(dimethylamino)phenyl)vinyl]phenoxy}-2-hydroxymethylpropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 902143-05-9
4-N,N'-dimethylamino-4'-(1,3-dihydroxypropane-2-ylmethoxy)stilbene

: 98-59-9
p-toluenesulfonyl chloride

: 902143-06-0
toluene-4-sulfonic acid 3-{4-[2-(4-(dimethylamino)phenyl)vinyl]phenoxy}-2-hydroxymethylpropyl ester

Guidance literature:: With pyridine; at 0 ℃; for 2h;
DOI:10.1021/jm050166g

Reference yield:

: 902143-04-8
4-N,N'-dimethylamino-4'-(2,2-dimethyl-[l,3]dioxane-5-ylmethoxy)stilbene

: 902143-06-0
toluene-4-sulfonic acid 3-{4-[2-(4-(dimethylamino)phenyl)vinyl]phenoxy}-2-hydroxymethylpropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / aq. HCl / acetone / 0 - 20 °C

2: 41 percent / pyridine / 2 h / 0 °C

With pyridine; hydrogenchloride; In acetone;
DOI:10.1021/jm050166g

Reference yield:

: 902143-06-0
toluene-4-sulfonic acid 3-{4-[2-(4-(dimethylamino)phenyl)vinyl]phenoxy}-2-hydroxymethylpropyl ester

: [18F]-3-{4-[2-(4-dimethylaminophenyl)vinyl]phenoxy}-2-fluoromethylpropan-1-ol

Guidance literature:: With hydrogen [¹⁸F]fluoride; potassium carbonate; In dimethyl sulfoxide; at 120 ℃; for 0.0666667h;
DOI:10.1021/jm050166g