4-O-acetyl-1,6-anhydro-2-benzyloxycarbonylamino-2,3-dideoxy-β-D-arabino-hexopyranose

Base Information

Chemical Name:4-O-acetyl-1,6-anhydro-2-benzyloxycarbonylamino-2,3-dideoxy-β-D-arabino-hexopyranose
CAS No.:92982-57-5
Molecular Formula:C₁₆H₁₉NO₆
Molecular Weight:321.33
Hs Code.:

Synonyms:4-O-acetyl-1,6-anhydro-2-benzyloxycarbonylamino-2,3-dideoxy-β-D-arabino-hexopyranose

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Chemical Property of 4-O-acetyl-1,6-anhydro-2-benzyloxycarbonylamino-2,3-dideoxy-β-D-arabino-hexopyranose

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Technology Process of 4-O-acetyl-1,6-anhydro-2-benzyloxycarbonylamino-2,3-dideoxy-β-D-arabino-hexopyranose

There total 6 articles about 4-O-acetyl-1,6-anhydro-2-benzyloxycarbonylamino-2,3-dideoxy-β-D-arabino-hexopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 92982-54-2
4-O-acetyl-1,6-anhydro-2-benzyloxycarbonylamino-2,3-dideoxy-3-iodo-β-D-mannopyranose

: 92982-57-5
4-O-acetyl-1,6-anhydro-2-benzyloxycarbonylamino-2,3-dideoxy-β-D-arabino-hexopyranose

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 0.166667h; Heating;
DOI:10.1016/0008-6215(84)85273-8

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 92982-57-5
4-O-acetyl-1,6-anhydro-2-benzyloxycarbonylamino-2,3-dideoxy-β-D-arabino-hexopyranose

Guidance literature:: Multi-step reaction with 6 steps

1: 89 percent / pyridine / 1.) -15 deg C, 2.) room temperature

2: 64 percent / pyridine / Ambient temperature

3: 80 percent / sodium methoxide / CHCl₃; methanol / 1 h / Ambient temperature

4: 1.1 g / sodium iodide / acetic acid / 0.08 h / 80 °C

5: pyridine / Ambient temperature

6: 75 percent / 2,2'-azobis(2-methylpropionitrile), tributyl stannane / benzene / 0.17 h / Heating

With pyridine; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium methylate; sodium iodide; In methanol; chloroform; acetic acid; benzene;
DOI:10.1016/0008-6215(84)85273-8

Reference yield:

: 92982-56-4
((1R,2R,3R,4R,5R)-2-Hydroxy-3-iodo-6,8-dioxa-bicyclo[3.2.1]oct-4-yl)-carbamic acid benzyl ester

: 92982-57-5
4-O-acetyl-1,6-anhydro-2-benzyloxycarbonylamino-2,3-dideoxy-β-D-arabino-hexopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / Ambient temperature

2: 75 percent / 2,2'-azobis(2-methylpropionitrile), tributyl stannane / benzene / 0.17 h / Heating

With pyridine; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene;
DOI:10.1016/0008-6215(84)85273-8